N1-<(3β,5β,12α)-3-benzylamino-12-hydroxy-cholan-24-yl>-N4-methylpiperazine

Base Information

Chemical Name:N1-<(3β,5β,12α)-3-benzylamino-12-hydroxy-cholan-24-yl>-N4-methylpiperazine
CAS No.:128625-37-6
Molecular Formula:C₃₆H₅₉N₃O
Molecular Weight:549.884
Hs Code.:

Synonyms:N1-<(3β,5β,12α)-3-benzylamino-12-hydroxy-cholan-24-yl>-N4-methylpiperazine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N1-<(3β,5β,12α)-3-benzylamino-12-hydroxy-cholan-24-yl>-N4-methylpiperazine

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Technology Process of N1-<(3β,5β,12α)-3-benzylamino-12-hydroxy-cholan-24-yl>-N4-methylpiperazine

There total 4 articles about N1-<(3β,5β,12α)-3-benzylamino-12-hydroxy-cholan-24-yl>-N4-methylpiperazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 125680-52-6
N₁<(3β, 5β)-3-Benzylamino-12,24-dioxo-cholan-24-yl> N₄-methylpiperazine

: 128625-37-6
N1-<(3β,5β,12α)-3-benzylamino-12-hydroxy-cholan-24-yl>-N4-methylpiperazine

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; for 20h; Heating;
DOI:10.1002/ardp.19903230404

Reference yield:

: 109-01-3
1-methyl-piperazine

: 128625-37-6
N1-<(3β,5β,12α)-3-benzylamino-12-hydroxy-cholan-24-yl>-N4-methylpiperazine

Guidance literature:: Multi-step reaction with 3 steps

1: 1) tributylamine, ethylchlorocarbonate / 1) dioxane, 10 min

2: NaBH₃CN / methanol / 48 h / Ambient temperature

3: 80 percent / LiAlH₄ / tetrahydrofuran / 20 h / Heating

With lithium aluminium tetrahydride; tributyl-amine; chloroformic acid ethyl ester; sodium cyanoborohydride; In tetrahydrofuran; methanol;
DOI:10.1002/ardp.19903230404

Reference yield:

: 2958-05-6
3,12-dioxo-7-deoxycholic acid

: 128625-37-6
N1-<(3β,5β,12α)-3-benzylamino-12-hydroxy-cholan-24-yl>-N4-methylpiperazine

Guidance literature:: Multi-step reaction with 3 steps

1: 1) tributylamine, ethylchlorocarbonate / 1) dioxane, 10 min

2: NaBH₃CN / methanol / 48 h / Ambient temperature

3: 80 percent / LiAlH₄ / tetrahydrofuran / 20 h / Heating

With lithium aluminium tetrahydride; tributyl-amine; chloroformic acid ethyl ester; sodium cyanoborohydride; In tetrahydrofuran; methanol;
DOI:10.1002/ardp.19903230404