1,5-anhydro-3,6-di-O-benzyl-4-O-methyl-2-deoxy-D-arabino-hex-1-wnopyranose

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Chemical Name:1,5-anhydro-3,6-di-O-benzyl-4-O-methyl-2-deoxy-D-arabino-hex-1-wnopyranose
CAS No.:145852-85-3
Molecular Formula:C₂₁H₂₄O₅
Molecular Weight:356.419
Hs Code.:

Synonyms:1,5-anhydro-3,6-di-O-benzyl-4-O-methyl-2-deoxy-D-arabino-hex-1-wnopyranose

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Chemical Property of 1,5-anhydro-3,6-di-O-benzyl-4-O-methyl-2-deoxy-D-arabino-hex-1-wnopyranose

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Technology Process of 1,5-anhydro-3,6-di-O-benzyl-4-O-methyl-2-deoxy-D-arabino-hex-1-wnopyranose

There total 1 articles about 1,5-anhydro-3,6-di-O-benzyl-4-O-methyl-2-deoxy-D-arabino-hex-1-wnopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 145852-77-3
1,5-anhydro-3,6-di-O-benzyl-4-O-methyl-2-deoxy-D-arabino-hex-1-enopyranose

: 145852-85-3
1,5-anhydro-3,6-di-O-benzyl-4-O-methyl-2-deoxy-D-arabino-hex-1-wnopyranose

Guidance literature:: With 3,3-dimethyldioxirane; In dichloromethane;
DOI:10.1016/S0968-0896(97)00094-1

Reference yield: 15.0%

: 195723-99-0
4-trifluoromethyl-3-toluidine hydroxyacetate

: 145852-85-3
1,5-anhydro-3,6-di-O-benzyl-4-O-methyl-2-deoxy-D-arabino-hex-1-wnopyranose

: 2-(3,6-di-O-benzyl-4-O-methyl-β-D-glucopyranosyl)-(3-methyl-4-trifluoromethyl-amidophenyl)oxyacetate

: 2-((2S,3S,4R,5S,6R)-6-Benzyloxymethyl-3,4-dihydroxy-5-methoxy-tetrahydro-pyran-2-yloxy)-N-(3-methyl-4-trifluoromethyl-phenyl)-acetamide

Guidance literature:: With sodium hydride; In tetrahydrofuran; for 3h; Ambient temperature;
DOI:10.1016/S0968-0896(97)00094-1

Reference yield:

: 145852-85-3
1,5-anhydro-3,6-di-O-benzyl-4-O-methyl-2-deoxy-D-arabino-hex-1-wnopyranose

: 1-<4-O-methyl-2,3,6-tris-O-(phenymethyl)-β-D-glucopyranosyl>-1H-indole

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) NaH / 1.) MeCN, room temperature, 45 min, 2.) MeCN, 50 deg C, 2 h; room temperature, overnight

2: 1.) NaH / 1.) THF, reflux, 1 h, 2.) reflux, overnight

With sodium hydride;
DOI:10.1021/jo982277b