methoxymethyl 6-β-<(p-nitrobenzyloxycarbonyl)methylsulfonamido>penicillinate sulfone

Base Information

Chemical Name:methoxymethyl 6-β-<(p-nitrobenzyloxycarbonyl)methylsulfonamido>penicillinate sulfone
CAS No.:159215-19-7
Molecular Formula:C₁₉H₂₃N₃O₁₂S₂
Molecular Weight:549.537
Hs Code.:

Synonyms:methoxymethyl 6-β-<(p-nitrobenzyloxycarbonyl)methylsulfonamido>penicillinate sulfone

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Chemical Property of methoxymethyl 6-β-<(p-nitrobenzyloxycarbonyl)methylsulfonamido>penicillinate sulfone

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Technology Process of methoxymethyl 6-β-<(p-nitrobenzyloxycarbonyl)methylsulfonamido>penicillinate sulfone

There total 3 articles about methoxymethyl 6-β-<(p-nitrobenzyloxycarbonyl)methylsulfonamido>penicillinate sulfone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 159215-15-3
methoxymethyl 6-β-<(p-nitrobenzyloxycarbonyl)methylsulfonamido>penicillinate

: 159215-19-7
methoxymethyl 6-β-<(p-nitrobenzyloxycarbonyl)methylsulfonamido>penicillinate sulfone

Guidance literature:: With potassium permanganate; acetic acid; In water; for 1h;
DOI:10.7164/antibiotics.47.1041

Reference yield:

: 619-73-8
4-nitrobenzyl chloride

: 159215-19-7
methoxymethyl 6-β-<(p-nitrobenzyloxycarbonyl)methylsulfonamido>penicillinate sulfone

Guidance literature:: Multi-step reaction with 3 steps

1: benzene / 1.5 h / Ambient temperature

2: 52.7 percent / Et₃N / CH₂Cl₂ / 0.5 h / Ambient temperature

3: 57 percent / KMnO₄, 80percent AcOH / H₂O / 1 h

With potassium permanganate; acetic acid; triethylamine; In dichloromethane; water; benzene;
DOI:10.7164/antibiotics.47.1041

Reference yield:

: 159215-11-9
p-nitrobenzyloxycarbonylmethylsulfonylchloride

: 159215-19-7
methoxymethyl 6-β-<(p-nitrobenzyloxycarbonyl)methylsulfonamido>penicillinate sulfone

Guidance literature:: Multi-step reaction with 2 steps

1: 52.7 percent / Et₃N / CH₂Cl₂ / 0.5 h / Ambient temperature

2: 57 percent / KMnO₄, 80percent AcOH / H₂O / 1 h

With potassium permanganate; acetic acid; triethylamine; In dichloromethane; water;
DOI:10.7164/antibiotics.47.1041