2-allyl-2-(N,N’-di-tert-butoxycarbonylhydrazino)malonic acid di-benzyl ester

Base Information

Chemical Name:2-allyl-2-(N,N’-di-tert-butoxycarbonylhydrazino)malonic acid di-benzyl ester
CAS No.:1618700-79-0
Molecular Formula:C₃₀H₃₈N₂O₈
Molecular Weight:554.64
Hs Code.:

Synonyms:2-allyl-2-(N,N’-di-tert-butoxycarbonylhydrazino)malonic acid di-benzyl ester

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Chemical Property of 2-allyl-2-(N,N’-di-tert-butoxycarbonylhydrazino)malonic acid di-benzyl ester

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Technology Process of 2-allyl-2-(N,N’-di-tert-butoxycarbonylhydrazino)malonic acid di-benzyl ester

There total 1 articles about 2-allyl-2-(N,N’-di-tert-butoxycarbonylhydrazino)malonic acid di-benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 870-50-8
di-tert-butyl-diazodicarboxylate

: 173541-54-3
dibenzyl 2-allylmalonate

: 1618700-79-0
2-allyl-2-(N,N’-di-tert-butoxycarbonylhydrazino)malonic acid di-benzyl ester

Guidance literature:: With sodium hydride; In tetrahydrofuran; at 20 ℃; for 0.25h; Inert atmosphere;
DOI:10.1080/00397911.2014.905601

Reference yield:

: 1618700-79-0
2-allyl-2-(N,N’-di-tert-butoxycarbonylhydrazino)malonic acid di-benzyl ester

: C₃₀H₄₀N₂O₉

Guidance literature:: 2-allyl-2-(N,N’-di-tert-butoxycarbonylhydrazino)malonic acid di-benzyl ester; With dimethylsulfide borane complex; In tetrahydrofuran; at 0 ℃; for 1.5h; Inert atmosphere;

With dihydrogen peroxide; sodium acetate; In tetrahydrofuran; water; for 1h;
DOI:10.1080/00397911.2014.905601

Reference yield:

: 1618700-79-0
2-allyl-2-(N,N’-di-tert-butoxycarbonylhydrazino)malonic acid di-benzyl ester

: C₃₁H₄₂N₂O₁₁S

Guidance literature:: Multi-step reaction with 2 steps

1.1: dimethylsulfide borane complex / tetrahydrofuran / 1.5 h / 0 °C / Inert atmosphere

1.2: 1 h

2.1: dmap; triethylamine / dichloromethane / 2 h / 0 °C / Inert atmosphere

With dmap; dimethylsulfide borane complex; triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1080/00397911.2014.905601