3-phenyl-3H-3-benzophosphenine pentacarbonylchromium⁽⁰⁾

Base Information

Chemical Name:3-phenyl-3H-3-benzophosphenine pentacarbonylchromium⁽⁰⁾
CAS No.:872599-99-0
Molecular Formula:C₂₁H₁₃CrO₅P
Molecular Weight:428.301
Hs Code.:

3-phenyl-3H-3-benzophosphenine pentacarbonylchromium<sup>(0)</sup>

Synonyms:3-phenyl-3H-3-benzophosphenine pentacarbonylchromium⁽⁰⁾

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Chemical Property of 3-phenyl-3H-3-benzophosphenine pentacarbonylchromium⁽⁰⁾

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Technology Process of 3-phenyl-3H-3-benzophosphenine pentacarbonylchromium⁽⁰⁾

There total 2 articles about 3-phenyl-3H-3-benzophosphenine pentacarbonylchromium⁽⁰⁾ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 39.0%

: 72868-71-4
phenylphosphine pentacarbonylchromium⁽⁰⁾

: 21792-52-9
1,2-diethynylbenzene

: 872599-99-0
3-phenyl-3H-3-benzophosphenine pentacarbonylchromium⁽⁰⁾

Guidance literature:: With KOH; In tetrahydrofuran; (N2); Cr complex and 1,2-diethynylbenzene dissolved in THF, KOH added after 2-3 h; filtered (silica), evapd., purified at 50°C under 1 mmHg, chromd.(toluene/pentane), crystd. from Et2O/pentane at -20°C;
DOI:10.1021/ja054885w