2,5-Dimethoxybenzaldehyde N-phenylthiosemicarbazone

Base Information

Chemical Name:2,5-Dimethoxybenzaldehyde N-phenylthiosemicarbazone
CAS No.:328044-97-9
Molecular Formula:C₁₆H₁₇N₃O₂S
Molecular Weight:315.396
Hs Code.:
European Community (EC) Number:669-286-8

Synonyms:STK262883;AKOS003237944;2,5-DIMETHOXYBENZALDEHYDE N-PHENYLTHIOSEMICARBAZONE;(2E)-2-(2,5-dimethoxybenzylidene)-N-phenylhydrazinecarbothioamide

Suppliers and Price of 2,5-Dimethoxybenzaldehyde N-phenylthiosemicarbazone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,5-Dimethoxybenzaldehyde N-phenylthiosemicarbazone

Chemical Property:

XLogP3:3.1
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:5
Exact Mass:315.10414797
Heavy Atom Count:22
Complexity:372

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:COC1=CC(=C(C=C1)OC)C=NNC(=S)NC2=CC=CC=C2
Isomeric SMILES:COC1=CC(=C(C=C1)OC)/C=N/NC(=S)NC2=CC=CC=C2

Technology Process of 2,5-Dimethoxybenzaldehyde N-phenylthiosemicarbazone

There total 1 articles about 2,5-Dimethoxybenzaldehyde N-phenylthiosemicarbazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 93-02-7
2,5-dimethoxybenzaldehyde

: 5351-69-9
4-Phenyl-3-thiosemicarbazide

: 328044-97-9
2,5-dimethoxybenzaldene-4-phenylthiosemicarbazone

Guidance literature:: With acetic acid; In ethanol; at 65 ℃; for 2h;
DOI:10.14233/ajchem.2018.21117

Reference yield: 82.0%

: 12107-56-1
dichloro(1,5-cyclooctadiene)palladium(II)

: 328044-97-9
2,5-dimethoxybenzaldene-4-phenylthiosemicarbazone

: C₃₂H₃₂N₆O₄PdS₂

Guidance literature:: In acetonitrile; at 20 ℃; for 3h;
DOI:10.14233/ajchem.2018.21117

Reference yield:

: 328044-97-9
2,5-dimethoxybenzaldene-4-phenylthiosemicarbazone

: 1380075-09-1
N¹-benzylidene-N²-[3-(2,5-dimethoxyphenyl)-4-(1,4-benzoquinon-2-yl)-1,3-thiazol-2-ylidene]hydrazine

Guidance literature:: Multi-step reaction with 2 steps

1: sodium acetate / ethanol / 18 h / Reflux

2: iron(III) chloride / water; N,N-dimethyl-formamide / 0.5 h

With iron(III) chloride; sodium acetate; In ethanol; water; N,N-dimethyl-formamide;
DOI:10.1007/s00044-012-0076-0