6-(([(2-hydroxy-3,5-dimethylphenyl)methyl](4-methoxyphenyl)amino)methyl)-2,4-dimethylphenol

Base Information

• Chemical Name: 6-(([(2-hydroxy-3,5-dimethylphenyl)methyl](4-methoxyphenyl)amino)methyl)-2,4-dimethylphenol
• CAS No.: 372524-14-6
• Molecular Formula: C₂₅H₂₉NO₃
• Molecular Weight: 391.51

Synonyms:6-(([(2-hydroxy-3,5-dimethylphenyl)methyl](4-methoxyphenyl)amino)methyl)-2,4-dimethylphenol

Chemical Property of 6-(([(2-hydroxy-3,5-dimethylphenyl)methyl](4-methoxyphenyl)amino)methyl)-2,4-dimethylphenol

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Technology Process of 6-(([(2-hydroxy-3,5-dimethylphenyl)methyl](4-methoxyphenyl)amino)methyl)-2,4-dimethylphenol

There total 1 articles about 6-(([(2-hydroxy-3,5-dimethylphenyl)methyl](4-methoxyphenyl)amino)methyl)-2,4-dimethylphenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-(6,8-dimethyl(2H,4H-benzo[e]1,3-oxazin-3-yl))-4-methoxybenzene (372524-12-4) + 2,4-Xylenol (105-67-9) → 6-[(1E)-2-(4-methoxyphenyl)-2-azavinyl]-2,4-dimethylphenol + 6-(([(2-hydroxy-3,5-dimethylphenyl)methyl](4-methoxyphenyl)amino)methyl)-2,4-dimethylphenol (372524-14-6)

Guidance literature:

With 1,10-decanedioic acid; at 150 ℃; for 1h; Neat (no solvent);

DOI:10.1021/ma901743h

Reference yield: 70.0%

propylphosphonic dichloride (4708-04-7) + 6-(([(2-hydroxy-3,5-dimethylphenyl)methyl](4-methoxyphenyl)amino)methyl)-2,4-dimethylphenol (372524-14-6) → 13-(4-methoxyphenyl)-2,4,8,10-tetramethyl-6-propyl-13,14-dihydro-12H-6λ5-dibenzo[d,i][1,3,7,2]dioxazaphosphecin-6-one (1352001-77-4)

Guidance literature:

With triethylamine; In toluene; at 0 - 50 ℃; for 5.33333h;

DOI:10.1002/jhet.727

Reference yield: 68.0%

butylphosphonic dichloride (2302-80-9) + 6-(([(2-hydroxy-3,5-dimethylphenyl)methyl](4-methoxyphenyl)amino)methyl)-2,4-dimethylphenol (372524-14-6) → 13-(4-methoxyphenyl)-2,4,8,10-tetramethyl-6-butyl-13,14-dihydro-12H-6λ5-dibenzo[d,i][1,3,7,2]dioxazaphosphecin-6-one (1352001-83-2)

Guidance literature:

With triethylamine; In toluene; at 0 - 50 ℃; for 5.33333h;

DOI:10.1002/jhet.727

upstream raw materials:

1-(6,8-dimethyl(2H,4H-benzo[e]1,3-oxazin-3-yl))-4-methoxybenzene

2,4-Xylenol

Downstream raw materials:

13-(4-methoxyphenyl)-2,4,8,10-tetramethyl-6-propyl-13,14-dihydro-12H-6λ5-dibenzo[d,i][1,3,7,2]dioxazaphosphecin-6-one

13-(4-methoxyphenyl)-2,4,8,10-tetramethyl-6-butyl-13,14-dihydro-12H-6λ5-dibenzo[d,i][1,3,7,2]dioxazaphosphecin-6-one

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