2-[4-(1,2,3,6-tetrahydro-pyridin-4-yl)-phenyl]-pyrimidine trifluoroacetate

Base Information

Chemical Name:2-[4-(1,2,3,6-tetrahydro-pyridin-4-yl)-phenyl]-pyrimidine trifluoroacetate
CAS No.:942190-01-4
Molecular Formula:C₂HF₃O₂*C₁₅H₁₅N₃
Molecular Weight:351.328
Hs Code.:

Synonyms:2-[4-(1,2,3,6-tetrahydro-pyridin-4-yl)-phenyl]-pyrimidine trifluoroacetate

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Chemical Property of 2-[4-(1,2,3,6-tetrahydro-pyridin-4-yl)-phenyl]-pyrimidine trifluoroacetate

Chemical Property:

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Technology Process of 2-[4-(1,2,3,6-tetrahydro-pyridin-4-yl)-phenyl]-pyrimidine trifluoroacetate

There total 3 articles about 2-[4-(1,2,3,6-tetrahydro-pyridin-4-yl)-phenyl]-pyrimidine trifluoroacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1056623-85-8
4-(4-pyrimidin-2-yl-phenyl)-piperidine-1-carboxylic acid tert-butyl ester

: 76-05-1
trifluoroacetic acid

: 942190-01-4
2-[4-(1,2,3,6-tetrahydro-pyridin-4-yl)-phenyl]-pyrimidine trifluoroacetate

Guidance literature:: In water; at 20 ℃; for 1h;

Reference yield:

: 80980-89-8
4-(4’-bromophenyl)piperidine

: 942190-01-4
2-[4-(1,2,3,6-tetrahydro-pyridin-4-yl)-phenyl]-pyrimidine trifluoroacetate

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / dmap / acetonitrile / 3 h / 20 °C

2: cesium fluoride / bis-tributylphosphine palladium⁽⁰⁾ / 1,4-dioxane / 90 °C

3: water / 1 h / 20 °C

With triethylamine; cesium fluoride; dmap; bis-tributylphosphine palladium⁽⁰⁾; In 1,4-dioxane; water; acetonitrile;

Reference yield:

: 769944-78-7
tert-butyl 4-(4-bromophenyl)piperidine-1-carboxylate

: 942190-01-4
2-[4-(1,2,3,6-tetrahydro-pyridin-4-yl)-phenyl]-pyrimidine trifluoroacetate

Guidance literature:: Multi-step reaction with 2 steps

1: cesium fluoride / bis-tributylphosphine palladium⁽⁰⁾ / 1,4-dioxane / 90 °C

2: water / 1 h / 20 °C

With cesium fluoride; bis-tributylphosphine palladium⁽⁰⁾; In 1,4-dioxane; water;