6-methyl-1-nitromethylcyclohexene

Base Information

• Chemical Name: 6-methyl-1-nitromethylcyclohexene
• CAS No.: 110890-74-9
• Molecular Formula: C₈H₁₃NO₂
• Molecular Weight: 155.197
• Mol file: 110890-74-9.mol

Synonyms:6-methyl-1-nitromethylcyclohexene

Chemical Property of 6-methyl-1-nitromethylcyclohexene

Chemical Property:

Purity/Quality:

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Technology Process of 6-methyl-1-nitromethylcyclohexene

There total 1 articles about 6-methyl-1-nitromethylcyclohexene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

nitromethane (75-52-5) + 2-Methylcyclohexanone (583-60-8) → 6-methyl-1-nitromethylcyclohexene (110890-74-9)

Guidance literature:

With ethylenediamine; Multistep reaction; 1.) 24 h, reflux, 2.) 200 deg C, 5 mmHg (bulb to bulb distillation);

DOI:10.1016/S0040-4020(01)89988-9

Reference yield: 64.0%

6-methyl-1-nitromethylcyclohexene (110890-74-9) → 2-methyl-cyclohexene-1-carboxaldehyde oxime (110890-75-0)

Guidance literature:

With carbon disulfide; triethylamine; In acetonitrile; for 1.5h; Ambient temperature;

DOI:10.1016/S0040-4020(01)89988-9

upstream raw materials:

nitromethane

2-Methylcyclohexanone

Downstream raw materials:

2-methyl-cyclohexene-1-carboxaldehyde oxime