C₃₃H₅₀O₅

Base Information

• Chemical Name: C₃₃H₅₀O₅
• CAS No.: 1350724-51-4
• Molecular Formula: C₃₃H₅₀O₅
• Molecular Weight: 526.757
• Mol file: 1350724-51-4.mol

Synonyms:C₃₃H₅₀O₅

Chemical Property of C₃₃H₅₀O₅

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₃H₅₀O₅

There total 4 articles about C₃₃H₅₀O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

C18H27BrO3 + 5-(1',1'-dimethyl-n-heptyl)-1,3-dihydroxybenzene (56469-10-4) → C33H50O5 (1350724-51-4)

Guidance literature:

5-(1',1'-dimethyl-n-heptyl)-1,3-dihydroxybenzene; With potassium fluoride; potassium carbonate; In acetone; for 0.5h; Reflux; Inert atmosphere;

C₁₈H₂₇BrO₃; In acetone; for 48h; Reflux; Inert atmosphere;

DOI:10.1021/jm200529h

Reference yield:

1,8-dibromooctane (4549-32-0) → C33H50O5 (1350724-51-4)

Guidance literature:

Multi-step reaction with 2 steps

1.1: sodium hydride / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere

1.2: Reflux; Inert atmosphere

2.1: potassium fluoride; potassium carbonate / acetone / 0.5 h / Reflux; Inert atmosphere

2.2: 48 h / Reflux; Inert atmosphere

With potassium fluoride; sodium hydride; potassium carbonate; In tetrahydrofuran; acetone;

DOI:10.1021/jm200529h

Reference yield:

1-(1',1'-dimethylheptyl)-3,5-dimethoxybenzene (60526-81-0) → C33H50O5 (1350724-51-4)

Guidance literature:

Multi-step reaction with 2 steps

1.1: boron tribromide / dichloromethane

2.1: potassium fluoride; potassium carbonate / acetone / 0.5 h / Reflux; Inert atmosphere

2.2: 48 h / Reflux; Inert atmosphere

With potassium fluoride; boron tribromide; potassium carbonate; In dichloromethane; acetone;

DOI:10.1021/jm200529h

upstream raw materials:

5-(1',1'-dimethyl-n-heptyl)-1,3-dihydroxybenzene

1,8-dibromooctane

1-(1',1'-dimethylheptyl)-3,5-dimethoxybenzene

cis-5-hydroxyl-2-phenyl-1,3-dioxane

Downstream raw materials:

2-{8-[3-hydroxy-5-(2-methyloctan-2-yl)phenoxy]octyloxy}propane-1,3-diol