C₅₀H₈₄O₇Si₂

Base Information

Chemical Name:C₅₀H₈₄O₇Si₂
CAS No.:1234064-59-5
Molecular Formula:C₅₀H₈₄O₇Si₂
Molecular Weight:853.384
Hs Code.:

C<sub>50</sub>H<sub>84</sub>O<sub>7</sub>Si<sub>2</sub>

Synonyms:C₅₀H₈₄O₇Si₂

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Chemical Property of C₅₀H₈₄O₇Si₂

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Technology Process of C₅₀H₈₄O₇Si₂

There total 31 articles about C₅₀H₈₄O₇Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 1234064-57-3
C₅₆H₉₈O₇Si₃

: 1234064-59-5
C₅₀H₈₄O₇Si₂

Guidance literature:: With pyridine; pyridine hydrofluoride; In tetrahydrofuran; for 0.75h;
DOI:10.1016/j.tet.2011.07.066

Reference yield:

: 1192350-68-7
(2R,3E)-4-iodo-2-methylbut-3-ene-1,2-diol

: 1234064-59-5
C₅₀H₈₄O₇Si₂

Guidance literature:: Multi-step reaction with 9 steps

1.1: 2,6-dimethylpyridine / dichloromethane / 1.5 h / -78 - 20 °C

2.1: pyridinium p-toluenesulfonate / methanol; dichloromethane / 0.25 h

3.1: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 1 h

4.1: tin(IV) chloride / dichloromethane / 0.75 h / -78 °C

4.2: 3 h / -78 °C

4.3: -78 - 20 °C

5.1: 2,6-dimethylpyridine / dichloromethane / 1.5 h / 0 - 20 °C

6.1: pyridine; pyridine hydrofluoride / tetrahydrofuran / 0.5 h

7.1: scandium tris(trifluoromethanesulfonate) / toluene / 3 h

8.1: tert.-butyl lithium; 9-methoxy-9-BBN / tetrahydrofuran; diethyl ether; hexane; pentane / 1.08 h / -78 - 20 °C

8.2: 20 °C

9.1: pyridine; pyridine hydrofluoride / tetrahydrofuran / 0.75 h

With pyridine; 2,6-dimethylpyridine; pyridine hydrofluoride; tert.-butyl lithium; pyridinium p-toluenesulfonate; tin(IV) chloride; sodium hydrogencarbonate; Dess-Martin periodane; 9-methoxy-9-BBN; scandium tris(trifluoromethanesulfonate); In tetrahydrofuran; methanol; diethyl ether; hexane; dichloromethane; toluene; pentane; 4.1: Sakurai reaction / 4.2: Sakurai reaction / 8.2: Suzuki-Miyaura coupling;
DOI:10.1016/j.tet.2011.07.066

Reference yield:

: 1192350-67-6
(4R)-4-((E)-2-iodovinyl)-2-(4-methoxyphenyl)-4-methyl-1,3-dioxolane

: 1234064-59-5
C₅₀H₈₄O₇Si₂

Guidance literature:: Multi-step reaction with 10 steps

1.1: pyridinium p-toluenesulfonate; toluene-4-sulfonic acid / methanol / 2 h

2.1: 2,6-dimethylpyridine / dichloromethane / 1.5 h / -78 - 20 °C

3.1: pyridinium p-toluenesulfonate / methanol; dichloromethane / 0.25 h

4.1: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 1 h

5.1: tin(IV) chloride / dichloromethane / 0.75 h / -78 °C

5.2: 3 h / -78 °C

5.3: -78 - 20 °C

6.1: 2,6-dimethylpyridine / dichloromethane / 1.5 h / 0 - 20 °C

7.1: pyridine; pyridine hydrofluoride / tetrahydrofuran / 0.5 h

8.1: scandium tris(trifluoromethanesulfonate) / toluene / 3 h

9.1: tert.-butyl lithium; 9-methoxy-9-BBN / tetrahydrofuran; diethyl ether; hexane; pentane / 1.08 h / -78 - 20 °C

9.2: 20 °C

10.1: pyridine; pyridine hydrofluoride / tetrahydrofuran / 0.75 h

With pyridine; 2,6-dimethylpyridine; pyridine hydrofluoride; tert.-butyl lithium; pyridinium p-toluenesulfonate; tin(IV) chloride; sodium hydrogencarbonate; Dess-Martin periodane; toluene-4-sulfonic acid; 9-methoxy-9-BBN; scandium tris(trifluoromethanesulfonate); In tetrahydrofuran; methanol; diethyl ether; hexane; dichloromethane; toluene; pentane; 5.1: Sakurai reaction / 5.2: Sakurai reaction / 9.2: Suzuki-Miyaura coupling;
DOI:10.1016/j.tet.2011.07.066