2-(4-aminosulfonyl-3-methoxyphenyl)-N-[1-(2-piperidinophenyl)-2-methylpropyl]acetamide

Base Information

Chemical Name:2-(4-aminosulfonyl-3-methoxyphenyl)-N-[1-(2-piperidinophenyl)-2-methylpropyl]acetamide
CAS No.:700359-74-6
Molecular Formula:C₂₄H₃₃N₃O₄S
Molecular Weight:459.61
Hs Code.:

Synonyms:2-(4-aminosulfonyl-3-methoxyphenyl)-N-[1-(2-piperidinophenyl)-2-methylpropyl]acetamide

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Chemical Property of 2-(4-aminosulfonyl-3-methoxyphenyl)-N-[1-(2-piperidinophenyl)-2-methylpropyl]acetamide

Chemical Property:

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Technology Process of 2-(4-aminosulfonyl-3-methoxyphenyl)-N-[1-(2-piperidinophenyl)-2-methylpropyl]acetamide

There total 5 articles about 2-(4-aminosulfonyl-3-methoxyphenyl)-N-[1-(2-piperidinophenyl)-2-methylpropyl]acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 700359-72-4
2-(4-aminosulfonyl-2-bromo-5-methoxyphenyl)-N-[1-(2-piperidinophenyl)-2-methyl-propyl]acetamide

: 700359-74-6
2-(4-aminosulfonyl-3-methoxyphenyl)-N-[1-(2-piperidinophenyl)-2-methylpropyl]acetamide

Guidance literature:: With ammonium formate; palladium on activated charcoal; In methanol; for 4h; Heating;
DOI:10.1081/SCC-120028635

Reference yield:

: 1798-09-0
m-methoxyphenylacetic acid

: 700359-74-6
2-(4-aminosulfonyl-3-methoxyphenyl)-N-[1-(2-piperidinophenyl)-2-methylpropyl]acetamide

Guidance literature:: Multi-step reaction with 5 steps

1: 95 percent / bromine / CH₂Cl₂ / 2 h / 20 °C

2: 52 percent / dicyclohexylcarbodiimide / toluene / 10 h / 20 °C

3: chlorosulfonic acid / CH₂Cl₂ / 5 h / Heating

4: NH₃ gas / CH₂Cl₂ / 0 °C

5: 90 percent / ammonium formate / Pd/C / methanol / 4 h / Heating

With chlorosulfonic acid; ammonia; bromine; ammonium formate; dicyclohexyl-carbodiimide; palladium on activated charcoal; In methanol; dichloromethane; toluene;
DOI:10.1081/SCC-120028635

Reference yield:

: 86826-93-9
2-(2-bromo-5-methoxyphenyl)acetic acid

: 700359-74-6
2-(4-aminosulfonyl-3-methoxyphenyl)-N-[1-(2-piperidinophenyl)-2-methylpropyl]acetamide

Guidance literature:: Multi-step reaction with 4 steps

1: 52 percent / dicyclohexylcarbodiimide / toluene / 10 h / 20 °C

2: chlorosulfonic acid / CH₂Cl₂ / 5 h / Heating

3: NH₃ gas / CH₂Cl₂ / 0 °C

4: 90 percent / ammonium formate / Pd/C / methanol / 4 h / Heating

With chlorosulfonic acid; ammonia; ammonium formate; dicyclohexyl-carbodiimide; palladium on activated charcoal; In methanol; dichloromethane; toluene;
DOI:10.1081/SCC-120028635