(S)-3-(2-hydrazinyl-2-oxoethyl)-5-methyl-N-((S)-1-phenylethyl) hexanamide

Base Information

Chemical Name:(S)-3-(2-hydrazinyl-2-oxoethyl)-5-methyl-N-((S)-1-phenylethyl) hexanamide
CAS No.:1310495-03-4
Molecular Formula:C₁₇H₂₇N₃O₂
Molecular Weight:305.42
Hs Code.:

Synonyms:(S)-3-(2-hydrazinyl-2-oxoethyl)-5-methyl-N-((S)-1-phenylethyl) hexanamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-3-(2-hydrazinyl-2-oxoethyl)-5-methyl-N-((S)-1-phenylethyl) hexanamide

Chemical Property:

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Technology Process of (S)-3-(2-hydrazinyl-2-oxoethyl)-5-methyl-N-((S)-1-phenylethyl) hexanamide

There total 6 articles about (S)-3-(2-hydrazinyl-2-oxoethyl)-5-methyl-N-((S)-1-phenylethyl) hexanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 1310495-02-3
(S)-ethyl 5-methyl-3-[2-oxo-2-((S)-1-phenylethylamino)ethyl] hexanoate

: 1310495-03-4
(S)-3-(2-hydrazinyl-2-oxoethyl)-5-methyl-N-((S)-1-phenylethyl) hexanamide

Guidance literature:: With hydrazine hydrate; In ethanol; for 4h; Reflux;

Reference yield:

: 1310495-01-2
3-isobutyl-4-((S)-1-phenylethylcarbamoyl)pentanedioic acid diethyl ester

: 1310495-03-4
(S)-3-(2-hydrazinyl-2-oxoethyl)-5-methyl-N-((S)-1-phenylethyl) hexanamide

Guidance literature:: Multi-step reaction with 2 steps

1: sodium chloride / water; dimethyl sulfoxide / 8 h / 145 - 155 °C

2: hydrazine hydrate / ethanol / 4 h / Reflux

With hydrazine hydrate; sodium chloride; In ethanol; water; dimethyl sulfoxide;

Reference yield:

: 2627-86-3
(S)-1-phenyl-ethylamine

: 1310495-03-4
(S)-3-(2-hydrazinyl-2-oxoethyl)-5-methyl-N-((S)-1-phenylethyl) hexanamide

Guidance literature:: Multi-step reaction with 4 steps

1.1: 2.5 h / 120 - 125 °C

2.1: sodium hydride / tetrahydrofuran / 1 h / 5 °C

2.2: 3.5 h / 5 - 20 °C

3.1: sodium chloride / water; dimethyl sulfoxide / 8 h / 145 - 155 °C

4.1: hydrazine hydrate / ethanol / 4 h / Reflux

With sodium hydride; hydrazine hydrate; sodium chloride; In tetrahydrofuran; ethanol; water; dimethyl sulfoxide;