N-(9-fluorenylmethoxycarbonyl)-O-[2-acetamido-3-O-benzyl-4,6-O-benzylidene-2-deoxy-α-D-galactopyranosyl]-L-threonine allyl ester

Base Information

• Chemical Name: N-(9-fluorenylmethoxycarbonyl)-O-[2-acetamido-3-O-benzyl-4,6-O-benzylidene-2-deoxy-α-D-galactopyranosyl]-L-threonine allyl ester
• CAS No.: 868259-93-2
• Molecular Formula: C₄₄H₄₆N₂O₁₀
• Molecular Weight: 762.857

Synonyms:N-(9-fluorenylmethoxycarbonyl)-O-[2-acetamido-3-O-benzyl-4,6-O-benzylidene-2-deoxy-α-D-galactopyranosyl]-L-threonine allyl ester

Chemical Property of N-(9-fluorenylmethoxycarbonyl)-O-[2-acetamido-3-O-benzyl-4,6-O-benzylidene-2-deoxy-α-D-galactopyranosyl]-L-threonine allyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-(9-fluorenylmethoxycarbonyl)-O-[2-acetamido-3-O-benzyl-4,6-O-benzylidene-2-deoxy-α-D-galactopyranosyl]-L-threonine allyl ester

There total 2 articles about N-(9-fluorenylmethoxycarbonyl)-O-[2-acetamido-3-O-benzyl-4,6-O-benzylidene-2-deoxy-α-D-galactopyranosyl]-L-threonine allyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-(9-fluorenylmethoxycarbonyl)-O-[2-azido-3-O-benzyl-4,6-O-benzylidene-2-deoxy-α-D-galactopyranosyl]-L-threonine allyl ester → N-(9-fluorenylmethoxycarbonyl)-O-[2-acetamido-3-O-benzyl-4,6-O-benzylidene-2-deoxy-α-D-galactopyranosyl]-L-threonine allyl ester (868259-93-2)

Guidance literature:

Multi-step reaction with 2 steps

1: Zn; AcOH / CH₂Cl₂ / 2 h

2: 83 mg / methanol; CH₂Cl₂ / 2 h

With acetic acid; zinc; In methanol; dichloromethane;

DOI:10.1021/ja053711b

Reference yield:

(2S,3R)-3-((2S,4aR,6S,7R,8R,8aR)-7-Amino-8-benzyloxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-6-yloxy)-2-(9H-fluoren-9-ylmethoxycarbonylamino)-butyric acid allyl ester + acetic anhydride (108-24-7) → N-(9-fluorenylmethoxycarbonyl)-O-[2-acetamido-3-O-benzyl-4,6-O-benzylidene-2-deoxy-α-D-galactopyranosyl]-L-threonine allyl ester (868259-93-2)

Guidance literature:

In methanol; dichloromethane; for 2h;

DOI:10.1021/ja053711b

Reference yield: 83.0%

N-(9-fluorenylmethoxycarbonyl)-O-[2-acetamido-3-O-benzyl-4,6-O-benzylidene-2-deoxy-α-D-galactopyranosyl]-L-threonine allyl ester (868259-93-2) → N-(9-fluorenylmethoxycarbonyl)-O-[2-acetamido-3-O-benzyl-4,6-O-benzylidene-2-deoxy-α-D-galactopyranosyl]-L-threonine (868259-92-1)

Guidance literature:

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; at 20 ℃; for 2h;

DOI:10.1021/ja053711b

upstream raw materials:

acetic anhydride

Downstream raw materials:

N-(9-fluorenylmethoxycarbonyl)-O-[2-acetamido-3-O-benzyl-4,6-O-benzylidene-2-deoxy-α-D-galactopyranosyl]-L-threonine

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 868259-93-2 N-(9-fluorenylmethoxycarbonyl)-O-[2-acetamido-3-O-benzyl-4,6-O-benzylidene-2-deoxy-α-D-galactopyranosyl]-L-threonine allyl ester

Send

Send

Metric Ton KG G Pound L ML

Send

Send