N-(benzyloxycarbonyl)-O-(3,4,6-tri-O-acetyl-2-azido-2-deoxy-α-D-galactopyranosyl)serine allyl ester

Base Information

Chemical Name:N-(benzyloxycarbonyl)-O-(3,4,6-tri-O-acetyl-2-azido-2-deoxy-α-D-galactopyranosyl)serine allyl ester
CAS No.:118417-95-1
Molecular Formula:C₂₆H₃₂N₄O₁₂
Molecular Weight:592.56
Hs Code.:

Synonyms:N-(benzyloxycarbonyl)-O-(3,4,6-tri-O-acetyl-2-azido-2-deoxy-α-D-galactopyranosyl)serine allyl ester

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Chemical Property of N-(benzyloxycarbonyl)-O-(3,4,6-tri-O-acetyl-2-azido-2-deoxy-α-D-galactopyranosyl)serine allyl ester

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Technology Process of N-(benzyloxycarbonyl)-O-(3,4,6-tri-O-acetyl-2-azido-2-deoxy-α-D-galactopyranosyl)serine allyl ester

There total 3 articles about N-(benzyloxycarbonyl)-O-(3,4,6-tri-O-acetyl-2-azido-2-deoxy-α-D-galactopyranosyl)serine allyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 67673-39-6
3,4,6-tri-O-acetyl-2-azido-2-deoxy-alpha-D-galactopyranosyl bromide

: 88295-41-4
N-(benzyloxycarbonyl)serine allyl ester

: 118417-95-1
N-(benzyloxycarbonyl)-O-(3,4,6-tri-O-acetyl-2-azido-2-deoxy-α-D-galactopyranosyl)serine allyl ester

Guidance literature:: With 2-methyl-1,2-epoxypropane; bathophenanthroline; In tert-butyl methyl ether; at 50 ℃; for 48h; stereoselective reaction; Schlenk technique; Sealed tube; Inert atmosphere;
DOI:10.1002/anie.201901346

Reference yield:

: 1145-80-8
N-(benzyloxycarbonyl)-L-serine

: 118417-95-1
N-(benzyloxycarbonyl)-O-(3,4,6-tri-O-acetyl-2-azido-2-deoxy-α-D-galactopyranosyl)serine allyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 83 percent / NaHCO₃, tricaprylmethylammonium chloride / H₂O; CH₂Cl₂ / 72 h

With Aliquat 336; sodium hydrogencarbonate; In dichloromethane; water;
DOI:10.1021/jo00265a007