(6R)-6-O-acetyl-2,3,4-tri-O-benzoyl-1,6-dideoxy-1,6-epithio-β-D-gluco-hexodialdo-1,5-pyranose

Base Information

Chemical Name:(6R)-6-O-acetyl-2,3,4-tri-O-benzoyl-1,6-dideoxy-1,6-epithio-β-D-gluco-hexodialdo-1,5-pyranose
CAS No.:300709-25-5
Molecular Formula:C₂₉H₂₄O₉S
Molecular Weight:548.57
Hs Code.:

Synonyms:(6R)-6-O-acetyl-2,3,4-tri-O-benzoyl-1,6-dideoxy-1,6-epithio-β-D-gluco-hexodialdo-1,5-pyranose

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (6R)-6-O-acetyl-2,3,4-tri-O-benzoyl-1,6-dideoxy-1,6-epithio-β-D-gluco-hexodialdo-1,5-pyranose

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Technology Process of (6R)-6-O-acetyl-2,3,4-tri-O-benzoyl-1,6-dideoxy-1,6-epithio-β-D-gluco-hexodialdo-1,5-pyranose

There total 2 articles about (6R)-6-O-acetyl-2,3,4-tri-O-benzoyl-1,6-dideoxy-1,6-epithio-β-D-gluco-hexodialdo-1,5-pyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 108-24-7
acetic anhydride

: 300709-14-2
2,3,4-tri-O-benzoyl-1,6-dideoxy-1,6-epithio-β-D-glucopyranose (S)-S-oxide

: 300709-25-5
(6R)-6-O-acetyl-2,3,4-tri-O-benzoyl-1,6-dideoxy-1,6-epithio-β-D-gluco-hexodialdo-1,5-pyranose

Guidance literature:: With sodium acetate; for 12h; Heating;
DOI:10.1071/ch99164

Reference yield:

: 189446-96-6
2,3,4-tri-O-benzoyl-1,6-dideoxy-1,6-epithio-β-D-glucopyranose

: 300709-25-5
(6R)-6-O-acetyl-2,3,4-tri-O-benzoyl-1,6-dideoxy-1,6-epithio-β-D-gluco-hexodialdo-1,5-pyranose

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / m-chloroperbenzoic acid / CH₂Cl₂ / 0.08 h / cooling

2: 91 percent / NaOAc / 12 h / Heating

With sodium acetate; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; 1: Oxidation / 2: Pummerer rearrangement;
DOI:10.1071/ch99164