1,2,3,4-tetrahydrobenzo-1,5-naphthyridine

Base Information

• Chemical Name: 1,2,3,4-tetrahydrobenzo-1,5-naphthyridine
• CAS No.: 106351-29-5
• Molecular Formula: C₁₂H₁₂N₂
• Molecular Weight: 184.241

Synonyms:1,2,3,4-tetrahydrobenzo-1,5-naphthyridine

Chemical Property of 1,2,3,4-tetrahydrobenzo-1,5-naphthyridine

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Technology Process of 1,2,3,4-tetrahydrobenzo-1,5-naphthyridine

There total 6 articles about 1,2,3,4-tetrahydrobenzo-1,5-naphthyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

1-[(2-methoxyphenyl)acetyl]-1,2,3,4-tetrahydrobenzo[c]-1,5-naphthyridine (116344-90-2) → 1,2,3,4-tetrahydrobenzo-1,5-naphthyridine (106351-29-5) + 1-[2-(2-Methoxy-phenyl)-ethyl]-1,2,3,4-tetrahydro-benzo[c][1,5]naphthyridine; hydrochloride (116345-08-5)

Guidance literature:

With hydrogenchloride; borane; In tetrahydrofuran; Ambient temperature;

DOI:10.1002/jhet.5570240609

Reference yield: 45.0%

1-[(2-fluorophenyl)acetyl]-1,2,3,4-tetrahydrobenzo[c]-1,5-naphthyridine (116344-88-8) → 1,2,3,4-tetrahydrobenzo-1,5-naphthyridine (106351-29-5) + 1-[2-(2-Fluorophenyl)ethyl]-1,2,3,4-tetrahydrobenzo[c]-1,5-naphthyridine hydrochloride (116345-06-3)

Guidance literature:

With hydrogenchloride; borane; In tetrahydrofuran; Ambient temperature;

DOI:10.1002/jhet.5570240609

Reference yield: 42.0%

1-[(2-chlorophenyl)acetyl]-1,2,3,4-tetrahydrobenzo[c]-1,5-naphthyridine (116344-89-9) → 1,2,3,4-tetrahydrobenzo-1,5-naphthyridine (106351-29-5) + 1-[2-(2-Chlorophenyl)ethyl]-1,2,3,4-tetrahydrobenzo[c]-1,5-naphthyridine hydrochloride (116345-07-4)

Guidance literature:

With hydrogenchloride; borane; In tetrahydrofuran; Ambient temperature;

DOI:10.1002/jhet.5570240609

upstream raw materials:

1-(Phenylacetyl)-1,2,3,4-tetrahydrobenzo[c]-1,5-naphthyridine

1-[(1-oxo-3-phenyl)propyl]-1,2,3,4-tetrahydrobenzo[c]-1,5-naphthyridine

1-[(4-chlorophenyl)acetyl]-1,2,3,4-tetrahydrobenzo[c]-1,5-naphthyridine

1-[(2-fluorophenyl)acetyl]-1,2,3,4-tetrahydrobenzo[c]-1,5-naphthyridine

Downstream raw materials:

1-benzoyl-1,2,3,4-tetrahydrobenzo-1,5-naphthyridine

1-[(4-chlorophenyl)acetyl]-1,2,3,4-tetrahydrobenzo[c]-1,5-naphthyridine

1-(Phenylacetyl)-1,2,3,4-tetrahydrobenzo[c]-1,5-naphthyridine

1-[(2-chlorophenyl)acetyl]-1,2,3,4-tetrahydrobenzo[c]-1,5-naphthyridine

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