1,3-di-tert-butyl-5-iodo-2-methoxy benzene

Base Information

Chemical Name:1,3-di-tert-butyl-5-iodo-2-methoxy benzene
CAS No.:71742-41-1
Molecular Formula:C₁₅H₂₃IO
Molecular Weight:346.252
Hs Code.:

Synonyms:1,3-di-tert-butyl-5-iodo-2-methoxy benzene

Suppliers and Price of 1,3-di-tert-butyl-5-iodo-2-methoxy benzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of 1,3-di-tert-butyl-5-iodo-2-methoxy benzene

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of 1,3-di-tert-butyl-5-iodo-2-methoxy benzene

There total 3 articles about 1,3-di-tert-butyl-5-iodo-2-methoxy benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1516-95-6
2,6-di-tert-butyl-anisole

: 71742-41-1
1,3-di-tert-butyl-5-iodo-2-methoxy benzene

Guidance literature:: With Iodine monochloride; In dichloromethane; at 0 ℃; for 1h;
DOI:10.1016/j.tet.2012.11.063

Reference yield:

: 128-39-2
2,6-di-tert-butylphenol

: 71742-41-1
1,3-di-tert-butyl-5-iodo-2-methoxy benzene

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) potassium t-butoxide / 1) DME, 1 h; 2) DME

2: 63 percent / iodine monochloride / CCl₄ / 1) 0 - 5 deg C; 2) room temperature, 2 h; 3) 50 deg C, 2 h

With potassium tert-butylate; Iodine monochloride; In tetrachloromethane;

Reference yield:

: 128-39-2
2,6-di-tert-butylphenol

: 71742-41-1
1,3-di-tert-butyl-5-iodo-2-methoxy benzene

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydride / N,N-dimethyl-formamide / 2 h / 0 °C

2: Iodine monochloride / dichloromethane / 1 h / 0 °C

With Iodine monochloride; sodium hydride; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.tet.2012.11.063