C₅₅H₈₁ClNO₁₁P

Base Information

Chemical Name:C₅₅H₈₁ClNO₁₁P
CAS No.:1422356-80-6
Molecular Formula:C₅₅H₈₁ClNO₁₁P
Molecular Weight:998.675
Hs Code.:

C<sub>55</sub>H<sub>81</sub>ClNO<sub>11</sub>P

Synonyms:C₅₅H₈₁ClNO₁₁P

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Chemical Property of C₅₅H₈₁ClNO₁₁P

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Technology Process of C₅₅H₈₁ClNO₁₁P

There total 22 articles about C₅₅H₈₁ClNO₁₁P which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.2%

: 1422355-59-6
4-((3aR,5aR,5bR,7aR,9S,11aR,11bR,13aS)-3a-(2-(1-(4-chlorophenyl)-cyclopropylamino)-2-oxoacetyl)-1-isopropyl-5a,5b,8,8,11a-pentamethyl-2-oxo-3,3a,4,5,5a,5b,6,7,7a,8,9,10,11,11a,11b,12,13,13a-octadecahydro-2H-cyclopenta[a]chrysen-9-yloxy)-2,2-dimethyl-4-oxobutanoic acid

: 229625-50-7
di-tert-butyl chloromethyl phosphate

: 1422356-80-6
C₅₅H₈₁ClNO₁₁P

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 50 ℃; for 4h;

Reference yield:

: 139255-65-5
((3aR,5aR,5bR,7aR,9S,11aR,11bR,13aS)-9-acetoxy-1-isopropyl-5a,5b,8,8,11a-pentamethyl-2-oxo-3,3a,4,5,5a,5b,6,7,7a,8,9,10,11,11a,11b,12,13,13a-octadecahydro-2H-cyclopenta[a]chrysen-3a-yl)methyl acetate

: 1422356-80-6
C₅₅H₈₁ClNO₁₁P

Guidance literature:: Multi-step reaction with 10 steps

1: potassium hydroxide / toluene; ethanol / 1 h / 20 °C

2: pyridinium chlorochromate / dichloromethane / 1 h / 20 °C

3: triethylamine / 20 °C

4: Dess-Martin periodane / dichloromethane / 2 h / 20 °C

5: acetic acid; sodium nitrite / dimethyl sulfoxide / 0 - 20 °C

6: N-ethyl-N,N-diisopropylamine; HATU / N,N-dimethyl-formamide / 1 h / 0 - 20 °C

7: hydrogenchloride; water / 20 - 45 °C

8: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap / dichloromethane / 1 h / 20 °C

9: trifluoroacetic acid / dichloromethane / 2 h / 20 °C

10: potassium carbonate / N,N-dimethyl-formamide / 4 h / 50 °C

With hydrogenchloride; dmap; water; potassium carbonate; Dess-Martin periodane; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-ethyl-N,N-diisopropylamine; HATU; pyridinium chlorochromate; trifluoroacetic acid; potassium hydroxide; sodium nitrite; In ethanol; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide; toluene;

Reference yield:

: 226384-14-1
(3aR,5aR,5bR,7aR,9S,11aR,11bR,13aS)-3a-(hydroxymethyl)-1-isopropyl-5a,5b,8, 8,11a-pentamethyl-2-oxo-3,3a,4,5,5a,5b,6,7,7a,8,9,10,11,11a,11b,12,13,13a-octadecahydro-2H-cyclopenta[a]chrysen-9-yl acetate

: 1422356-80-6
C₅₅H₈₁ClNO₁₁P

Guidance literature:: Multi-step reaction with 12 steps

1.1: pyridinium chlorochromate / dichloromethane / 1 h / 20 °C

2.1: n-butyllithium / tetrahydrofuran; hexane / 2 h / -40 - -20 °C / Inert atmosphere

2.2: 1 h / -78 - -70 °C / Inert atmosphere

3.1: triethylamine; dmap / dichloromethane / 2 h / 20 - 50 °C

4.1: N-Bromosuccinimide / acetonitrile; water / 0.17 h / 20 °C

5.1: 2-methyl-but-2-ene; sodium chlorite; sodium dihydrogenphosphate / tetrahydrofuran; water; tert-butyl alcohol / 0.92 h / 0 - 20 °C

6.1: potassium hydroxide / toluene; ethanol / 0.5 h / 20 °C

7.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dimethyl sulfoxide / 3 h / 50 °C

8.1: N-ethyl-N,N-diisopropylamine; HATU / N,N-dimethyl-formamide / 1 h / 0 - 20 °C

9.1: hydrogenchloride; water / 20 - 45 °C

10.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap / dichloromethane / 1 h / 20 °C

11.1: trifluoroacetic acid / dichloromethane / 2 h / 20 °C

12.1: potassium carbonate / N,N-dimethyl-formamide / 4 h / 50 °C

With hydrogenchloride; dmap; sodium chlorite; sodium dihydrogenphosphate; N-Bromosuccinimide; n-butyllithium; 2-methyl-but-2-ene; water; potassium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-ethyl-N,N-diisopropylamine; HATU; pyridinium chlorochromate; trifluoroacetic acid; potassium hydroxide; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; ethanol; hexane; dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide; toluene; acetonitrile; tert-butyl alcohol;