(Z)-3-(2-Phenyl-[1,3]oxathiolan-2-ylmethoxy)-thioacrylic acid S-methyl ester

Base Information

• Chemical Name: (Z)-3-(2-Phenyl-[1,3]oxathiolan-2-ylmethoxy)-thioacrylic acid S-methyl ester
• CAS No.: 88640-38-4
• Molecular Formula: C₁₄H₁₆O₃S₂
• Molecular Weight: 296.411

Synonyms:(Z)-3-(2-Phenyl-[1,3]oxathiolan-2-ylmethoxy)-thioacrylic acid S-methyl ester

Chemical Property of (Z)-3-(2-Phenyl-[1,3]oxathiolan-2-ylmethoxy)-thioacrylic acid S-methyl ester

Chemical Property:

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Technology Process of (Z)-3-(2-Phenyl-[1,3]oxathiolan-2-ylmethoxy)-thioacrylic acid S-methyl ester

There total 1 articles about (Z)-3-(2-Phenyl-[1,3]oxathiolan-2-ylmethoxy)-thioacrylic acid S-methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(E)-3-Methanesulfinyl-thioacrylic acid S-methyl ester (88640-33-9) + Lithium; (2-phenyl-[1,3]oxathiolan-2-yl)-methanolate (88640-41-9) → (Z)-3-(2-Phenyl-[1,3]oxathiolan-2-ylmethoxy)-thioacrylic acid S-methyl ester (88640-38-4)

Guidance literature:

In tetrahydrofuran;

DOI:10.1016/S0040-4039(00)94141-8

Reference yield: 81.0%

(Z)-3-(2-Phenyl-[1,3]oxathiolan-2-ylmethoxy)-thioacrylic acid S-methyl ester (88640-38-4) → (Z)-3-(2-Oxo-2-phenyl-ethoxy)-thioacrylic acid S-methyl ester (88640-39-5)

Guidance literature:

With chloroamine-T; In water; acetonitrile; at 25 ℃; for 1h;

DOI:10.1016/S0040-4039(00)94141-8

upstream raw materials:

(E)-3-Methanesulfinyl-thioacrylic acid S-methyl ester

Lithium; (2-phenyl-[1,3]oxathiolan-2-yl)-methanolate

Downstream raw materials:

(Z)-3-(2-Oxo-2-phenyl-ethoxy)-thioacrylic acid S-methyl ester

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