Technology Process of C37H35BrO5
There total 8 articles about C37H35BrO5 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
triethylamine;
In
dichloromethane;
at 20 ℃;
for 1.75h;
Inert atmosphere;
DOI:10.1016/j.tet.2011.04.094
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: potassium tert-butylate / tetrahydrofuran / 0.5 h / -20 - -15 °C / Inert atmosphere; Cooling with acetone-dry ice
1.2: 0.25 h / -15 - 20 °C / Inert atmosphere
2.1: AD-mix-β; water / tert-butyl alcohol / 2 h / 20 °C / Inert atmosphere
3.1: triethylamine / dichloromethane / 1.75 h / 20 °C / Inert atmosphere
With
AD-mix-β; potassium tert-butylate; water; triethylamine;
In
tetrahydrofuran; dichloromethane; tert-butyl alcohol;
2.1: Sharpless dihydroxylation;
DOI:10.1016/j.tet.2011.04.094
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: caesium carbonate; sodium iodide / N,N-dimethyl-formamide / 0.33 h / 20 °C / Inert atmosphere
2.1: potassium tert-butylate / tetrahydrofuran / 0.5 h / -20 - -15 °C / Inert atmosphere; Cooling with acetone-dry ice
2.2: 0.25 h / -15 - 20 °C / Inert atmosphere
3.1: AD-mix-β; water / tert-butyl alcohol / 2 h / 20 °C / Inert atmosphere
4.1: triethylamine / dichloromethane / 1.75 h / 20 °C / Inert atmosphere
With
AD-mix-β; potassium tert-butylate; water; caesium carbonate; triethylamine; sodium iodide;
In
tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; tert-butyl alcohol;
3.1: Sharpless dihydroxylation;
DOI:10.1016/j.tet.2011.04.094
