6,6,6-triphenylhexanenitrile

Base Information

Chemical Name:6,6,6-triphenylhexanenitrile
CAS No.:33885-07-3
Molecular Formula:C₂₄H₂₃N
Molecular Weight:325.453
Hs Code.:

Synonyms:6,6,6-triphenylhexanenitrile

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Chemical Property of 6,6,6-triphenylhexanenitrile

Chemical Property:

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Technology Process of 6,6,6-triphenylhexanenitrile

There total 3 articles about 6,6,6-triphenylhexanenitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 61883-36-1
(E)-pent-3-ene-1,1,1-triyltribenzene

: 1-methylcyclohexa-2,5-diene-1-carbonitrile

: 33885-07-3
6,6,6-triphenylhexanenitrile

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; tris(pentafluorophenyl)borate; 4,5-bis(diphenylphos4,5-bis(diphenylphosphino)-9,9-dimethylxanthenephino)-9,9-dimethylxanthene; In 1,4-dioxane; at 110 ℃; for 40h; regioselective reaction; Glovebox; Inert atmosphere;
DOI:10.1021/jacs.8b10651

Reference yield:

: 76-83-5
trityl chloride

: 33885-07-3
6,6,6-triphenylhexanenitrile

Guidance literature:: Multi-step reaction with 2 steps

1: (i) Na-Hg, (ii) /BRN= 635673/

2: NaI

With sodium iodide;
DOI:10.1021/jo00974a001