Technology Process of C33H30O7Si
There total 5 articles about C33H30O7Si which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
sodium phosphate dibasic dodecahydrate; 3-chloro-benzenecarboperoxoic acid;
In
1,2-dichloro-ethane;
at 20 - 50 ℃;
for 3h;
DOI:10.1002/chem.201300702
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: n-butyllithium / diethyl ether; hexane / 1 h / -78 °C / Inert atmosphere
1.2: 1 h / -78 - 20 °C / Inert atmosphere
2.1: [RuCl2(p-cymene)2]; water / acetonitrile / 20 °C
3.1: {1,3-bis[2,6-bis(1-methylethyl)phenyl]-1,3-dihydro-2H-imidazol-2-ylidene}(methyl)gold; C51H57F3NO5PS / toluene / 36 h / 25 °C / Inert atmosphere
4.1: 3-chloro-benzenecarboperoxoic acid; sodium phosphate dibasic dodecahydrate / 1,2-dichloro-ethane / 3 h / 20 - 50 °C
With
n-butyllithium; sodium phosphate dibasic dodecahydrate; [RuCl2(p-cymene)2]; {1,3-bis[2,6-bis(1-methylethyl)phenyl]-1,3-dihydro-2H-imidazol-2-ylidene}(methyl)gold; C51H57F3NO5PS; water; 3-chloro-benzenecarboperoxoic acid;
In
diethyl ether; hexane; 1,2-dichloro-ethane; toluene; acetonitrile;
3.1: |Mukaiyama Aldol Addition / 4.1: |Baeyer-Villiger Ketone Oxidation;
DOI:10.1002/chem.201300702
- Guidance literature:
-
Multi-step reaction with 3 steps
1: [RuCl2(p-cymene)2]; water / acetonitrile / 20 °C
2: {1,3-bis[2,6-bis(1-methylethyl)phenyl]-1,3-dihydro-2H-imidazol-2-ylidene}(methyl)gold; C51H57F3NO5PS / toluene / 36 h / 25 °C / Inert atmosphere
3: 3-chloro-benzenecarboperoxoic acid; sodium phosphate dibasic dodecahydrate / 1,2-dichloro-ethane / 3 h / 20 - 50 °C
With
sodium phosphate dibasic dodecahydrate; [RuCl2(p-cymene)2]; {1,3-bis[2,6-bis(1-methylethyl)phenyl]-1,3-dihydro-2H-imidazol-2-ylidene}(methyl)gold; C51H57F3NO5PS; water; 3-chloro-benzenecarboperoxoic acid;
In
1,2-dichloro-ethane; toluene; acetonitrile;
2: |Mukaiyama Aldol Addition / 3: |Baeyer-Villiger Ketone Oxidation;
DOI:10.1002/chem.201300702