1-hydroxy-8-methoxy-2-(3-oxo-3-phenylpropionyl)anthraquinone

Base Information

• Chemical Name: 1-hydroxy-8-methoxy-2-(3-oxo-3-phenylpropionyl)anthraquinone
• CAS No.: 1017590-46-3
• Molecular Formula: C₂₄H₁₆O₆
• Molecular Weight: 400.387
• Mol file: 1017590-46-3.mol

Synonyms:1-hydroxy-8-methoxy-2-(3-oxo-3-phenylpropionyl)anthraquinone

Chemical Property of 1-hydroxy-8-methoxy-2-(3-oxo-3-phenylpropionyl)anthraquinone

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of 1-hydroxy-8-methoxy-2-(3-oxo-3-phenylpropionyl)anthraquinone

There total 1 articles about 1-hydroxy-8-methoxy-2-(3-oxo-3-phenylpropionyl)anthraquinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-acetyl-8-methoxy-9,10-dihydro-anthracen-1-yl benzoate (1017590-41-8) → 1-hydroxy-8-methoxy-2-(3-oxo-3-phenylpropionyl)anthraquinone (1017590-46-3)

Guidance literature:

With lithium hydride; In tetrahydrofuran; for 20h; Heating;

DOI:10.1016/j.bmcl.2007.12.055

Reference yield: 94.0%

1-hydroxy-8-methoxy-2-(3-oxo-3-phenylpropionyl)anthraquinone (1017590-46-3) → C24H14O5 (1017590-51-0)

Guidance literature:

With trifluoroacetic acid; at 0 - 20 ℃; for 0.833333h;

DOI:10.1016/j.bmcl.2007.12.055

Reference yield:

1-hydroxy-8-methoxy-2-(3-oxo-3-phenylpropionyl)anthraquinone (1017590-46-3) → 11-hydroxy-2-phenylanthra[1,2-b]pyran-4,7,12-trione

Guidance literature:

With hydrogen bromide; acetic acid; for 8h; Heating;

DOI:10.1016/j.bmcl.2007.12.055

upstream raw materials:

2-acetyl-8-methoxy-9,10-dihydro-anthracen-1-yl benzoate

Downstream raw materials:

C₂₄H₁₄O₅