ethyl (1S,2R,3S,5R)-2-benzamido-3,5-diphenethylcyclopentanecarboxylate

Base Information

Chemical Name:ethyl (1S,2R,3S,5R)-2-benzamido-3,5-diphenethylcyclopentanecarboxylate
CAS No.:1446558-40-2
Molecular Formula:C₃₁H₃₅NO₃
Molecular Weight:469.624
Hs Code.:

Synonyms:ethyl (1S,2R,3S,5R)-2-benzamido-3,5-diphenethylcyclopentanecarboxylate

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Chemical Property of ethyl (1S,2R,3S,5R)-2-benzamido-3,5-diphenethylcyclopentanecarboxylate

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Technology Process of ethyl (1S,2R,3S,5R)-2-benzamido-3,5-diphenethylcyclopentanecarboxylate

There total 8 articles about ethyl (1S,2R,3S,5R)-2-benzamido-3,5-diphenethylcyclopentanecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 1446558-38-8
ethyl (1S,2R,3R,5S)-2-benzamido-3,5-di((E)-styryl)cyclopentanecarboxylate

: 1446558-40-2
ethyl (1S,2R,3S,5R)-2-benzamido-3,5-diphenethylcyclopentanecarboxylate

Guidance literature:: With 5%-palladium/activated carbon; hydrogen; In ethyl acetate; at 20 ℃; for 1h;
DOI:10.1002/chem.201203183

Reference yield:

: 14735-70-7,14805-31-3,924272-78-6,670221-11-1
diexo-3-Aza-4-oxotricyclo<4.2.1.0^2,5>non-7-ene

: 1446558-40-2
ethyl (1S,2R,3S,5R)-2-benzamido-3,5-diphenethylcyclopentanecarboxylate

Guidance literature:: Multi-step reaction with 7 steps

1.1: water / 168 h / 70 °C / Enzymatic reaction

2.1: hydrogenchloride / 0 °C

3.1: sodium hydrogencarbonate / toluene / 0 °C

4.1: 4-methylmorpholine N-oxide; osmium(VIII) oxide / acetone / 12 h / 20 °C

5.1: sodium periodate / water; tetrahydrofuran / 0.17 h / 20 °C / Inert atmosphere

6.1: potassium tert-butylate / tetrahydrofuran / 0.17 h / 0 °C

6.2: 1 h / 20 °C

7.1: 5%-palladium/activated carbon; hydrogen / ethyl acetate / 1 h / 20 °C

With hydrogenchloride; sodium periodate; osmium(VIII) oxide; 5%-palladium/activated carbon; potassium tert-butylate; water; hydrogen; sodium hydrogencarbonate; 4-methylmorpholine N-oxide; In tetrahydrofuran; water; ethyl acetate; acetone; toluene; 6.2: |Wittig Rearrangement;
DOI:10.1002/chem.201203183

Reference yield:

: 924272-78-6,670221-11-1
(1R,2R,5S,6S)-3-azatricyclo[4.2.1.0^2,5]non-7-en-4-one

: 1446558-40-2
ethyl (1S,2R,3S,5R)-2-benzamido-3,5-diphenethylcyclopentanecarboxylate

Guidance literature:: Multi-step reaction with 6 steps

1.1: hydrogenchloride / 0 °C

2.1: sodium hydrogencarbonate / toluene / 0 °C

3.1: 4-methylmorpholine N-oxide; osmium(VIII) oxide / acetone / 12 h / 20 °C

4.1: sodium periodate / water; tetrahydrofuran / 0.17 h / 20 °C / Inert atmosphere

5.1: potassium tert-butylate / tetrahydrofuran / 0.17 h / 0 °C

5.2: 1 h / 20 °C

6.1: 5%-palladium/activated carbon; hydrogen / ethyl acetate / 1 h / 20 °C

With hydrogenchloride; sodium periodate; osmium(VIII) oxide; 5%-palladium/activated carbon; potassium tert-butylate; hydrogen; sodium hydrogencarbonate; 4-methylmorpholine N-oxide; In tetrahydrofuran; water; ethyl acetate; acetone; toluene; 5.2: |Wittig Rearrangement;
DOI:10.1002/chem.201203183