N-(4-{5-[(1,4-benzodioxan-2-yl)methylsulfanyl]-1,3,4-thiadiazol-2-yl}phenyl)-3-bromobenzamide

Base Information

Chemical Name:N-(4-{5-[(1,4-benzodioxan-2-yl)methylsulfanyl]-1,3,4-thiadiazol-2-yl}phenyl)-3-bromobenzamide
CAS No.:1608151-09-2
Molecular Formula:C₂₄H₁₈BrN₃O₃S₂
Molecular Weight:540.461
Hs Code.:

Synonyms:N-(4-{5-[(1,4-benzodioxan-2-yl)methylsulfanyl]-1,3,4-thiadiazol-2-yl}phenyl)-3-bromobenzamide

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Chemical Property of N-(4-{5-[(1,4-benzodioxan-2-yl)methylsulfanyl]-1,3,4-thiadiazol-2-yl}phenyl)-3-bromobenzamide

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Technology Process of N-(4-{5-[(1,4-benzodioxan-2-yl)methylsulfanyl]-1,3,4-thiadiazol-2-yl}phenyl)-3-bromobenzamide

There total 2 articles about N-(4-{5-[(1,4-benzodioxan-2-yl)methylsulfanyl]-1,3,4-thiadiazol-2-yl}phenyl)-3-bromobenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 2164-34-3
2-(bromomethyl)-2,3-dihydrobenzo[1,4]dioxine

: 885906-10-5
3-bromo-N-[4-(5-sulfanyl-1,3,4-thiadiazol-2-yl)-phenyl]benzamide

: 1608151-09-2
N-(4-{5-[(1,4-benzodioxan-2-yl)methylsulfanyl]-1,3,4-thiadiazol-2-yl}phenyl)-3-bromobenzamide

Guidance literature:: 3-bromo-N-[4-(5-sulfanyl-1,3,4-thiadiazol-2-yl)-phenyl]benzamide; With potassium hydroxide; In ethanol; at 50 - 60 ℃; for 0.5h;

2-(bromomethyl)-2,3-dihydrobenzo[1,4]dioxine; In ethanol; Reflux;
DOI:10.1134/S1070428014030233

Reference yield:

: 5351-17-7
4-aminobenzohydrazide

: 1608151-09-2
N-(4-{5-[(1,4-benzodioxan-2-yl)methylsulfanyl]-1,3,4-thiadiazol-2-yl}phenyl)-3-bromobenzamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium hydroxide / ethanol / 35 - 40 °C

1.2: -2 - 0 °C

2.1: pyridine / benzene / Reflux

3.1: potassium hydroxide / ethanol / 0.5 h / 50 - 60 °C

3.2: Reflux

With pyridine; potassium hydroxide; In ethanol; benzene;
DOI:10.1134/S1070428014030233