C₂₈H₃₀O₆S

Base Information

Chemical Name:C₂₈H₃₀O₆S
CAS No.:1256640-05-7
Molecular Formula:C₂₈H₃₀O₆S
Molecular Weight:494.609
Hs Code.:

C<sub>28</sub>H<sub>30</sub>O<sub>6</sub>S

Synonyms:C₂₈H₃₀O₆S

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Chemical Property of C₂₈H₃₀O₆S

Chemical Property:

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Technology Process of C₂₈H₃₀O₆S

There total 13 articles about C₂₈H₃₀O₆S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 1256640-04-6
C₂₈H₃₂O₇S

: 1256640-05-7
C₂₈H₃₀O₆S

Guidance literature:: C₂₈H₃₂O₇S; With lithium perchlorate; In dichloromethane; at 20 ℃; for 0.75h; Molecular sieve; Inert atmosphere;

With bismuth(lll) trifluoromethanesulfonate; In dichloromethane; at 20 ℃; for 3.5h; diastereoselective reaction; Inert atmosphere;
DOI:10.1021/ol102390t

Reference yield:

: 1256640-02-4
C₂₉H₃₄O₆S

: 1256640-05-7
C₂₈H₃₀O₆S

Guidance literature:: Multi-step reaction with 3 steps

1.1: osmium(VIII) oxide; 4-methylmorpholine N-oxide / tetrahydrofuran; water; tert-butyl alcohol / 12 h / 20 °C

2.1: sodium periodate / tetrahydrofuran; water / 2 h / 20 °C

3.1: lithium perchlorate / dichloromethane / 0.75 h / 20 °C / Molecular sieve; Inert atmosphere

3.2: 3.5 h / 20 °C / Inert atmosphere

With sodium periodate; osmium(VIII) oxide; lithium perchlorate; 4-methylmorpholine N-oxide; In tetrahydrofuran; dichloromethane; water; tert-butyl alcohol; 3.1: Friedel Crafts acylation / 3.2: Friedel Crafts acylation;
DOI:10.1021/ol102390t

Reference yield:

: 1256640-00-2
C₁₉H₂₂O₄

: 1256640-05-7
C₂₈H₃₀O₆S

Guidance literature:: Multi-step reaction with 5 steps

1.1: tetrahydrofuran / 1.83 h / -40 - 20 °C / Inert atmosphere

2.1: di(n-butyl)tin oxide; triethylamine / dichloromethane / 3 h / 20 °C / Inert atmosphere

3.1: osmium(VIII) oxide; 4-methylmorpholine N-oxide / tetrahydrofuran; water; tert-butyl alcohol / 12 h / 20 °C

4.1: sodium periodate / tetrahydrofuran; water / 2 h / 20 °C

5.1: lithium perchlorate / dichloromethane / 0.75 h / 20 °C / Molecular sieve; Inert atmosphere

5.2: 3.5 h / 20 °C / Inert atmosphere

With sodium periodate; osmium(VIII) oxide; lithium perchlorate; di(n-butyl)tin oxide; 4-methylmorpholine N-oxide; triethylamine; In tetrahydrofuran; dichloromethane; water; tert-butyl alcohol; 5.1: Friedel Crafts acylation / 5.2: Friedel Crafts acylation;
DOI:10.1021/ol102390t