Co(H)2(P(CH₂CH₂P(C₆H₅)2)3)⁽¹⁺⁾*PF₆^(1-)=[Co(H)2(P(CH₂CH₂P(C₆H₅)2)3)]PF₆

Base Information

• Chemical Name: Co(H)2(P(CH₂CH₂P(C₆H₅)2)3)⁽¹⁺⁾*PF₆^(1-)=[Co(H)2(P(CH₂CH₂P(C₆H₅)2)3)]PF₆
• CAS No.: 184486-18-8
• Molecular Formula: C₄₂H₄₄CoP₄*F₆P
• Molecular Weight: 876.664
• Mol file: 184486-18-8.mol

Synonyms:Co(H)2(P(CH₂CH₂P(C₆H₅)2)3)⁽¹⁺⁾*PF₆^(1-)=[Co(H)2(P(CH₂CH₂P(C₆H₅)2)3)]PF₆

Chemical Property of Co(H)2(P(CH₂CH₂P(C₆H₅)2)3)⁽¹⁺⁾*PF₆^(1-)=[Co(H)2(P(CH₂CH₂P(C₆H₅)2)3)]PF₆

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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Useful:

Technology Process of Co(H)2(P(CH₂CH₂P(C₆H₅)2)3)⁽¹⁺⁾*PF₆^(1-)=[Co(H)2(P(CH₂CH₂P(C₆H₅)2)3)]PF₆

There total 1 articles about Co(H)2(P(CH₂CH₂P(C₆H₅)2)3)⁽¹⁺⁾*PF₆^(1-)=[Co(H)2(P(CH₂CH₂P(C₆H₅)2)3)]PF₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

HPF6*Et2O (4590-57-2) + P(CH2CH2P(C6H5)2)3CoH (55088-11-4) → Co(H)2(P(CH2CH2P(C6H5)2)3)(1+)*PF6(1-)=[Co(H)2(P(CH2CH2P(C6H5)2)3)]PF6 (184486-18-8)

Guidance literature:

In diethyl ether; (Ar or N2); addn. of HPF6 to Co(I) complex until the supernatant was colorless; filtration;

DOI:10.1021/ja962702n

Reference yield:

Co(H)2(P(CH2CH2P(C6H5)2)3)(1+)*PF6(1-)=[Co(H)2(P(CH2CH2P(C6H5)2)3)]PF6 (184486-18-8) + deuterium (16873-17-9,12184-84-8) → P(CH2CH2P(C6H5)2)3CoH(2)H(1+)*PF6(1-)=[P(CH2CH2P(C6H5)2)3CoH(2)H]*PF6

Guidance literature:

In acetone; (Ar or N2); frozen sample was put under D2;

DOI:10.1021/ja962702n

upstream raw materials:

HPF₆*Et₂O

P(CH₂CH₂P(C₆H₅)2)3CoH