pentafluorophenyl 2-phenyl-3-methylbutanoate

Base Information

Chemical Name:pentafluorophenyl 2-phenyl-3-methylbutanoate
CAS No.:1093959-80-8
Molecular Formula:C₁₇H₁₃F₅O₂
Molecular Weight:344.281
Hs Code.:

Synonyms:pentafluorophenyl 2-phenyl-3-methylbutanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of pentafluorophenyl 2-phenyl-3-methylbutanoate

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Technology Process of pentafluorophenyl 2-phenyl-3-methylbutanoate

There total 1 articles about pentafluorophenyl 2-phenyl-3-methylbutanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 771-61-9
2,3,4,5,6-pentafluorophenol

: 3508-94-9
3-methyl-2-phenylbutyric acid

: 1093959-80-8
pentafluorophenyl 2-phenyl-3-methylbutanoate

Guidance literature:: 2,3,4,5,6-pentafluorophenol; With dicyclohexyl-carbodiimide; In dichloromethane; for 0.0333333h; Inert atmosphere;

3-methyl-2-phenylbutyric acid; In dichloromethane; for 14h; Inert atmosphere;
DOI:10.1016/j.tetasy.2011.02.021

Reference yield: 51.0%

: 1093959-80-8
pentafluorophenyl 2-phenyl-3-methylbutanoate

: 190970-57-1
(S)-4-phenyl-1,3-oxazolidine-2-thione

: 1169704-44-2
C₂₀H₂₁NO₂S

: C₂₀H₂₁NO₂S

Guidance literature:: (S)-4-phenyl-1,3-oxazolidine-2-thione; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃;

pentafluorophenyl 2-phenyl-3-methylbutanoate; In tetrahydrofuran; hexane; at -78 - 20 ℃; for 12h; optical yield given as %de; diastereoselective reaction;
DOI:10.1055/s-0028-1088218

Reference yield: 25.0%

: 1093959-80-8
pentafluorophenyl 2-phenyl-3-methylbutanoate

: 62941-94-0
ethyl (+/-)-2-oxooxazolidine-4-carboxylate

: ethyl (rac)-syn-2-oxa-3-[2-phenyl-3-methylbutanoyl]oxazolidin-4-carboxylate

: ethyl (rac)-anti-2-oxa-3-[2-phenyl-3-methylbutanoyl]oxazolidin-4-carboxylate

Guidance literature:: ethyl (+/-)-2-oxooxazolidine-4-carboxylate; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 1h; Inert atmosphere;

pentafluorophenyl 2-phenyl-3-methylbutanoate; In tetrahydrofuran; hexane; at -78 ℃; for 2h; optical yield given as %de; diastereoselective reaction; Inert atmosphere;
DOI:10.1016/j.tetasy.2011.02.021