3-(2-methoxyphenyl)but-2-en-1-ol

Base Information

Chemical Name:3-(2-methoxyphenyl)but-2-en-1-ol
CAS No.:1240592-93-1
Molecular Formula:C₁₁H₁₄O₂
Molecular Weight:178.231
Hs Code.:

Synonyms:3-(2-methoxyphenyl)but-2-en-1-ol

Suppliers and Price of 3-(2-methoxyphenyl)but-2-en-1-ol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-(2-methoxyphenyl)but-2-en-1-ol

Chemical Property:

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Technology Process of 3-(2-methoxyphenyl)but-2-en-1-ol

There total 1 articles about 3-(2-methoxyphenyl)but-2-en-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 7706-84-5
3-(2-methoxy-phenyl)-crotonic acid ethyl ester

: 1240592-93-1
3-(2-methoxyphenyl)but-2-en-1-ol

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; at 0 - 20 ℃; Inert atmosphere; Schlenk technique;
DOI:10.1039/c8cc03017k

Reference yield:

: 1240592-93-1
3-(2-methoxyphenyl)but-2-en-1-ol

: C₁₁H₁₄O₄

Guidance literature:: With oxygen; methylene blue; In acetonitrile; at -10 - 0 ℃; for 10h;
DOI:10.1021/ci100180e

Reference yield:

: 1240592-93-1
3-(2-methoxyphenyl)but-2-en-1-ol

: C₁₁H₁₃FO₂

: C₁₁H₁₃FO₂

Guidance literature:: 3-(2-methoxyphenyl)but-2-en-1-ol; With disodium hydrogenphosphate; ethyl-cyclohexane; C₆₄H₇₃O₄P; 4-methylphenylboronic acid; magnesium sulfate; In para-xylene; at 20 ℃; for 1h; Sealed tube;

With Selectfluor; In para-xylene; at 20 ℃; for 36h; Overall yield = 83 %; enantioselective reaction; Sealed tube;
DOI:10.1021/ja507468u