Methyl 5-iodo-2,6-dioxo-1,2,3,6-tetrahydro-4-pyrimidinecarboxylate

Base Information

• Chemical Name: Methyl 5-iodo-2,6-dioxo-1,2,3,6-tetrahydro-4-pyrimidinecarboxylate
• CAS No.: 116393-71-6
• Molecular Formula: C₆H₅IN₂O₄
• Molecular Weight: 296.021

Synonyms:5-iodo methyl orotate

Chemical Property of Methyl 5-iodo-2,6-dioxo-1,2,3,6-tetrahydro-4-pyrimidinecarboxylate

Chemical Property:

• Melting Point: 283-285°
• PKA: 3.49±0.10(Predicted)
• Density: 2.17±0.1 g/cm3(Predicted)

Purity/Quality:

97% ^*data from raw suppliers

Methyl 5-iodo-2,6-dioxo-1,2,3,6-tetrahydro-4-pyrimidinecarboxylate >95% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Methyl 5-iodo-2,6-dioxo-1,2,3,6-tetrahydro-4-pyrimidinecarboxylate

There total 1 articles about Methyl 5-iodo-2,6-dioxo-1,2,3,6-tetrahydro-4-pyrimidinecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

methyl orotate (6153-44-2) → 5-iodo methyl orotate (116393-71-6)

Guidance literature:

With iodine; periodic acid; In methanol; for 20h; Heating / reflux;

Reference yield: 48.0%

5-iodo methyl orotate (116393-71-6) → 2,6-Dichloro-5-iodopyrimidine-4-carboxylic acid methyl ester (1136962-00-9)

Guidance literature:

With trichlorophosphate; N,N-dimethyl-formamide; for 3h; Heating / reflux;

Reference yield: 46.0%

2,4-dihydroxy-5-iodo-6-methoxycarbonylpyrimidine (116393-71-6) → 2,6-Dichloro-5-iodopyrimidine-4-carboxylic acid methyl ester (1136962-00-9)

Guidance literature:

With trichlorophosphate; N,N-dimethyl-formamide; for 3h; Reflux;

upstream raw materials:

methyl orotate

Downstream raw materials:

2,6-Dichloro-5-iodopyrimidine-4-carboxylic acid methyl ester

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