4'-(4'''-cyanophenyl)-1,2':6',1''-bispyrazolylpyridine

Base Information

Chemical Name:4'-(4'''-cyanophenyl)-1,2':6',1''-bispyrazolylpyridine
CAS No.:951663-83-5
Molecular Formula:C₁₈H₁₂N₆
Molecular Weight:312.333
Hs Code.:

Synonyms:4'-(4'''-cyanophenyl)-1,2':6',1''-bispyrazolylpyridine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4'-(4'''-cyanophenyl)-1,2':6',1''-bispyrazolylpyridine

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Technology Process of 4'-(4'''-cyanophenyl)-1,2':6',1''-bispyrazolylpyridine

There total 1 articles about 4'-(4'''-cyanophenyl)-1,2':6',1''-bispyrazolylpyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 918959-37-2
4-iodo-2,6-bis(1H-pyrazol-1-yl)pyridine

: 126747-14-6
4-cyanophenylboronic acid

: 951663-83-5
4'-(4'''-cyanophenyl)-1,2':6',1''-bispyrazolylpyridine

Guidance literature:: With sodium carbonate; In methanol; toluene; at 70 ℃; for 48h;
DOI:10.1039/b703700g

Reference yield:

: 951663-83-5
4'-(4'''-cyanophenyl)-1,2':6',1''-bispyrazolylpyridine

: iron(II) perchlorate hexahydrate

: 75-05-8,26809-02-9
acetonitrile

: [Fe(II)(4'-(4'''-cyanophenyl)-1,2':6',1''-bispyrazolylpyridine)2](ClO₄)2*2CH₃CN

Guidance literature:: In acetonitrile; (Schlenk); soln. of ligand and Fe(ClO4)2*6H2O in MeCN heated at 80°C for 6 h, cooled to room temp.; diisopropyl ether added under N2 at room temp.; elem. anal.;
DOI:10.1039/b703700g