Technology Process of C20H14O6
There total 4 articles about C20H14O6 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
boron tribromide;
In
dichloromethane;
at -78 ℃;
for 2h;
Inert atmosphere;
DOI:10.1016/j.bmc.2012.11.037
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: n-butyllithium / tetrahydrofuran; hexane / 0.33 h / -78 °C / Inert atmosphere
1.2: 3 h / -78 - 20 °C / Inert atmosphere
2.1: acetic anhydride; acetic acid / dichloromethane / 24 h / 140 °C / Inert atmosphere
3.1: sodium tetrahydroborate / tetrahydrofuran / 2 h / 20 °C / Inert atmosphere
4.1: boron tribromide / dichloromethane / 2 h / -78 °C / Inert atmosphere
With
sodium tetrahydroborate; n-butyllithium; acetic anhydride; boron tribromide; acetic acid;
In
tetrahydrofuran; hexane; dichloromethane;
2.1: |Diels-Alder Cycloaddition;
DOI:10.1016/j.bmc.2012.11.037
- Guidance literature:
-
Multi-step reaction with 3 steps
1: acetic anhydride; acetic acid / dichloromethane / 24 h / 140 °C / Inert atmosphere
2: sodium tetrahydroborate / tetrahydrofuran / 2 h / 20 °C / Inert atmosphere
3: boron tribromide / dichloromethane / 2 h / -78 °C / Inert atmosphere
With
sodium tetrahydroborate; acetic anhydride; boron tribromide; acetic acid;
In
tetrahydrofuran; dichloromethane;
1: |Diels-Alder Cycloaddition;
DOI:10.1016/j.bmc.2012.11.037
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