O-(4-(3,5-dimethoxy-4-propoxybenzyl)-7-ethoxyisoquinolin-8-yl) dimethylcarbamothioate

Base Information

Chemical Name:O-(4-(3,5-dimethoxy-4-propoxybenzyl)-7-ethoxyisoquinolin-8-yl) dimethylcarbamothioate
CAS No.:1351593-56-0
Molecular Formula:C₂₆H₃₂N₂O₅S
Molecular Weight:484.616
Hs Code.:

Synonyms:O-(4-(3,5-dimethoxy-4-propoxybenzyl)-7-ethoxyisoquinolin-8-yl) dimethylcarbamothioate

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Chemical Property of O-(4-(3,5-dimethoxy-4-propoxybenzyl)-7-ethoxyisoquinolin-8-yl) dimethylcarbamothioate

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Technology Process of O-(4-(3,5-dimethoxy-4-propoxybenzyl)-7-ethoxyisoquinolin-8-yl) dimethylcarbamothioate

There total 6 articles about O-(4-(3,5-dimethoxy-4-propoxybenzyl)-7-ethoxyisoquinolin-8-yl) dimethylcarbamothioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1351592-44-3
4-(3,5-dimethoxy-4-propoxybenzyl)-7-ethoxyisoquinolin-8-ol

: 16420-13-6
N,N-Dimethylthiocarbamoyl chloride

: 1351593-56-0
O-(4-(3,5-dimethoxy-4-propoxybenzyl)-7-ethoxyisoquinolin-8-yl) dimethylcarbamothioate

Guidance literature:: With potassium hydroxide; In tetrahydrofuran; water; at 4 - 20 ℃; for 1.66667h;

Reference yield:

: 492-88-6
3-ethoxysalicylaldehyde

: 1351593-56-0
O-(4-(3,5-dimethoxy-4-propoxybenzyl)-7-ethoxyisoquinolin-8-yl) dimethylcarbamothioate

Guidance literature:: Multi-step reaction with 4 steps

1: toluene / 4 h / 150 °C / Inert atmosphere

2: ethanol; sodium tetrahydroborate / 1 h / 100 °C / Inert atmosphere

3: hydrogenchloride / ethanol; water / 0.42 h / 90 °C

4: potassium hydroxide / water; tetrahydrofuran / 1.67 h / 4 - 20 °C

With hydrogenchloride; sodium tetrahydroborate; ethanol; potassium hydroxide; In tetrahydrofuran; ethanol; water; toluene;

Reference yield:

: 134-96-3
syringic aldehyde

: 1351593-56-0
O-(4-(3,5-dimethoxy-4-propoxybenzyl)-7-ethoxyisoquinolin-8-yl) dimethylcarbamothioate

Guidance literature:: Multi-step reaction with 3 steps

1: caesium carbonate / N,N-dimethyl-formamide / 10 h / 40 °C / Inert atmosphere

2: hydrogenchloride / ethanol; water / 0.42 h / 90 °C

3: potassium hydroxide / water; tetrahydrofuran / 1.67 h / 4 - 20 °C

With hydrogenchloride; caesium carbonate; potassium hydroxide; In tetrahydrofuran; ethanol; water; N,N-dimethyl-formamide;