1-(4-benzyloxy-2-tert-butoxycarbonylbutyl)cyclohex-2-ene carboxylic acid

Base Information

Chemical Name:1-(4-benzyloxy-2-tert-butoxycarbonylbutyl)cyclohex-2-ene carboxylic acid
CAS No.:219121-23-0
Molecular Formula:C₂₃H₃₂O₅
Molecular Weight:388.504
Hs Code.:

Synonyms:1-(4-benzyloxy-2-tert-butoxycarbonylbutyl)cyclohex-2-ene carboxylic acid

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Chemical Property of 1-(4-benzyloxy-2-tert-butoxycarbonylbutyl)cyclohex-2-ene carboxylic acid

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Technology Process of 1-(4-benzyloxy-2-tert-butoxycarbonylbutyl)cyclohex-2-ene carboxylic acid

There total 1 articles about 1-(4-benzyloxy-2-tert-butoxycarbonylbutyl)cyclohex-2-ene carboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 219121-22-9
2-(2-benzyloxyethyl)acrylic acid tert-butyl ester

: C₇H₈O₂^(2-)*2Li⁽¹⁺⁾

: 219121-23-0
1-(4-benzyloxy-2-tert-butoxycarbonylbutyl)cyclohex-2-ene carboxylic acid

: 2,4-Bis-(2-benzyloxy-ethyl)-4-tert-butoxycarbonyl-6-isobutyl-heptanedioic acid 1-tert-butyl ester

Guidance literature:: In tetrahydrofuran; at -78 ℃;
DOI:10.1016/0960-894X(96)00304-6

Reference yield:

: 219121-23-0
1-(4-benzyloxy-2-tert-butoxycarbonylbutyl)cyclohex-2-ene carboxylic acid

: 2-(1-Benzylcarbamoyl-cyclohexylmethyl)-4-(1,3-dioxo-1,3-dihydro-benzo[f]isoindol-2-yl)-butyric acid

Guidance literature:: Multi-step reaction with 4 steps

1: DEC, HOBT, Et₃N / CH₂Cl₂

2: H₂ / Pd(OH)2/C / acetic acid

3: PPh₃, DEAD / tetrahydrofuran

4: TFA

With diethylcarbamazine; hydrogen; benzotriazol-1-ol; triethylamine; triphenylphosphine; trifluoroacetic acid; diethylazodicarboxylate; palladium dihydroxide; In tetrahydrofuran; dichloromethane; acetic acid;
DOI:10.1016/0960-894X(96)00304-6

Reference yield:

: 219121-23-0
1-(4-benzyloxy-2-tert-butoxycarbonylbutyl)cyclohex-2-ene carboxylic acid

: 4-Hydroxy-2-[1-(2-morpholin-4-yl-ethylcarbamoyl)-cyclohexylmethyl]-butyric acid tert-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: DEC, HOBT, Et₃N / CH₂Cl₂

2: H₂ / Pd(OH)2/C / acetic acid

With diethylcarbamazine; hydrogen; benzotriazol-1-ol; triethylamine; palladium dihydroxide; In dichloromethane; acetic acid;
DOI:10.1016/0960-894X(96)00304-6