[(S)-1-(3-Benzyloxy-4-methoxy-phenyl)-2-(2-methyl-[1,3]dioxolan-2-yl)-ethyl]-[(E)-5-benzyloxy-pent-2-en-(E)-ylidene]-amine

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Chemical Name:[(S)-1-(3-Benzyloxy-4-methoxy-phenyl)-2-(2-methyl-[1,3]dioxolan-2-yl)-ethyl]-[(E)-5-benzyloxy-pent-2-en-(E)-ylidene]-amine
CAS No.:851755-93-6
Molecular Formula:C₃₂H₃₇NO₅
Molecular Weight:515.649
Hs Code.:

Synonyms:[(S)-1-(3-Benzyloxy-4-methoxy-phenyl)-2-(2-methyl-[1,3]dioxolan-2-yl)-ethyl]-[(E)-5-benzyloxy-pent-2-en-(E)-ylidene]-amine

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Chemical Property of [(S)-1-(3-Benzyloxy-4-methoxy-phenyl)-2-(2-methyl-[1,3]dioxolan-2-yl)-ethyl]-[(E)-5-benzyloxy-pent-2-en-(E)-ylidene]-amine

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Technology Process of [(S)-1-(3-Benzyloxy-4-methoxy-phenyl)-2-(2-methyl-[1,3]dioxolan-2-yl)-ethyl]-[(E)-5-benzyloxy-pent-2-en-(E)-ylidene]-amine

There total 7 articles about [(S)-1-(3-Benzyloxy-4-methoxy-phenyl)-2-(2-methyl-[1,3]dioxolan-2-yl)-ethyl]-[(E)-5-benzyloxy-pent-2-en-(E)-ylidene]-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 851755-92-5
(S)-1-(3-Benzyloxy-4-methoxy-phenyl)-2-(2-methyl-[1,3]dioxolan-2-yl)-ethylamine

: (E)-5-(benzyloxy)pent-2-enal

: 851755-93-6
[(S)-1-(3-Benzyloxy-4-methoxy-phenyl)-2-(2-methyl-[1,3]dioxolan-2-yl)-ethyl]-[(E)-5-benzyloxy-pent-2-en-(E)-ylidene]-amine

Guidance literature:: In chloroform; at 20 ℃;
DOI:10.1016/j.tetlet.2005.02.110

Reference yield:

: 851755-89-0
(S)-1-(3-Benzyloxy-4-methoxy-phenyl)-but-3-enylamine

: 851755-93-6
[(S)-1-(3-Benzyloxy-4-methoxy-phenyl)-2-(2-methyl-[1,3]dioxolan-2-yl)-ethyl]-[(E)-5-benzyloxy-pent-2-en-(E)-ylidene]-amine

Guidance literature:: Multi-step reaction with 5 steps

1: 87 percent / toluene / Heating

2: 86 percent / O₂ / PdCl₂; CuCl₂ / H₂O; dimethylformamide / 85 °C

3: TsOH / benzene / Heating

4: (NH₂)2*H₂O / ethanol / Heating

5: 100 percent / CHCl₃ / 20 °C

With oxygen; toluene-4-sulfonic acid; hydrazine hydrate; copper dichloride; palladium dichloride; In ethanol; chloroform; water; N,N-dimethyl-formamide; toluene; benzene; 2: Wacker oxidation;
DOI:10.1016/j.tetlet.2005.02.110

Reference yield:

: 851755-87-8
3-benzyloxy-4-methoxy-benzaldehyde O-(2-hydroxy-2-naphthalen-2-yl-ethyl)-oxime

: 851755-93-6
[(S)-1-(3-Benzyloxy-4-methoxy-phenyl)-2-(2-methyl-[1,3]dioxolan-2-yl)-ethyl]-[(E)-5-benzyloxy-pent-2-en-(E)-ylidene]-amine

Guidance literature:: Multi-step reaction with 7 steps

1: diethyl ether; toluene / 0.33 h / 45 °C

2: 82 percent / Zn; AcOH / tetrahydrofuran; H₂O / 60 °C

3: 87 percent / toluene / Heating

4: 86 percent / O₂ / PdCl₂; CuCl₂ / H₂O; dimethylformamide / 85 °C

5: TsOH / benzene / Heating

6: (NH₂)2*H₂O / ethanol / Heating

7: 100 percent / CHCl₃ / 20 °C

With oxygen; toluene-4-sulfonic acid; hydrazine hydrate; acetic acid; zinc; copper dichloride; palladium dichloride; In tetrahydrofuran; diethyl ether; ethanol; chloroform; water; N,N-dimethyl-formamide; toluene; benzene; 4: Wacker oxidation;
DOI:10.1016/j.tetlet.2005.02.110