C₅₈H₆₄N₉O₈P

Base Information

Chemical Name:C₅₈H₆₄N₉O₈P
CAS No.:1137726-82-9
Molecular Formula:C₅₈H₆₄N₉O₈P
Molecular Weight:1046.18
Hs Code.:

C<sub>58</sub>H<sub>64</sub>N<sub>9</sub>O<sub>8</sub>P

Synonyms:C₅₈H₆₄N₉O₈P

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Chemical Property of C₅₈H₆₄N₉O₈P

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Technology Process of C₅₈H₆₄N₉O₈P

There total 10 articles about C₅₈H₆₄N₉O₈P which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 2-cyanoethyl bis(diisopropylamino)phosphite

: 8-[acetyl(2-fluorenyl)amino]-5'-O-dimethoxytrityl-N²-[(dimethylamino)methylene]-2'-deoxyguanosine

: 1137726-82-9
C₅₈H₆₄N₉O₈P

Guidance literature:: With 4,5-dicyano-1H-imidazole; In dichloromethane; acetonitrile; at 20 ℃; Inert atmosphere;
DOI:10.1002/ejoc.201200984

Reference yield:

: 607-57-8
2-nitro-9H-fluorene

: 1137726-82-9
C₅₈H₆₄N₉O₈P

Guidance literature:: Multi-step reaction with 7 steps

1: hydrazine hydrate / ethanol / 0 °C

2: sodium hydrogencarbonate / diethyl ether / 0 °C

3: caesium carbonate / 1,2-dimethoxyethane / 20 °C / Inert atmosphere

4: tetrabutyl ammonium fluoride; acetic acid / tetrahydrofuran

5: pyridine / 20 °C / Inert atmosphere

6: pyridine / 20 °C / Inert atmosphere

7: 4,5-dicyano-1H-imidazole / dichloromethane; acetonitrile / 20 °C / Inert atmosphere

With pyridine; 4,5-dicyano-1H-imidazole; tetrabutyl ammonium fluoride; sodium hydrogencarbonate; caesium carbonate; hydrazine hydrate; acetic acid; In tetrahydrofuran; 1,2-dimethoxyethane; diethyl ether; ethanol; dichloromethane; acetonitrile;
DOI:10.1002/ejoc.201200984

Reference yield:

: 53-94-1
N-(9H-fluoren-2-yl)hydroxylamine

: 1137726-82-9
C₅₈H₆₄N₉O₈P

Guidance literature:: Multi-step reaction with 6 steps

1: sodium hydrogencarbonate / diethyl ether / 0 °C

2: caesium carbonate / 1,2-dimethoxyethane / 20 °C / Inert atmosphere

3: tetrabutyl ammonium fluoride; acetic acid / tetrahydrofuran

4: pyridine / 20 °C / Inert atmosphere

5: pyridine / 20 °C / Inert atmosphere

6: 4,5-dicyano-1H-imidazole / dichloromethane; acetonitrile / 20 °C / Inert atmosphere

With pyridine; 4,5-dicyano-1H-imidazole; tetrabutyl ammonium fluoride; sodium hydrogencarbonate; caesium carbonate; acetic acid; In tetrahydrofuran; 1,2-dimethoxyethane; diethyl ether; dichloromethane; acetonitrile;
DOI:10.1002/ejoc.201200984