tert-butyl 5-(4-(3-(2-(methoxy(methoxycarbonyl)amino)benzyloxy)-1H-pyrazol-1-yl)phenylthio)pentanoate

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Chemical Name:tert-butyl 5-(4-(3-(2-(methoxy(methoxycarbonyl)amino)benzyloxy)-1H-pyrazol-1-yl)phenylthio)pentanoate
CAS No.:1284183-81-8
Molecular Formula:C₂₈H₃₅N₃O₆S
Molecular Weight:541.668
Hs Code.:

Synonyms:tert-butyl 5-(4-(3-(2-(methoxy(methoxycarbonyl)amino)benzyloxy)-1H-pyrazol-1-yl)phenylthio)pentanoate

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Chemical Property of tert-butyl 5-(4-(3-(2-(methoxy(methoxycarbonyl)amino)benzyloxy)-1H-pyrazol-1-yl)phenylthio)pentanoate

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Technology Process of tert-butyl 5-(4-(3-(2-(methoxy(methoxycarbonyl)amino)benzyloxy)-1H-pyrazol-1-yl)phenylthio)pentanoate

There total 6 articles about tert-butyl 5-(4-(3-(2-(methoxy(methoxycarbonyl)amino)benzyloxy)-1H-pyrazol-1-yl)phenylthio)pentanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 151827-83-7
methyl N-(2-bromomethylphenyl)-N-methoxy-carbamate

: 1284183-77-2
tert-butyl 5-(4-(3-hydroxy-1H-pyrazol-1-yl)phenylthio)pentanoate

: 1284183-81-8
tert-butyl 5-(4-(3-(2-(methoxy(methoxycarbonyl)amino)benzyloxy)-1H-pyrazol-1-yl)phenylthio)pentanoate

Guidance literature:: With caesium carbonate; In N,N-dimethyl-formamide; at 20 ℃; Inert atmosphere;
DOI:10.1039/c0ob00686f

Reference yield:

: 1284183-71-6
1-(4-iodophenyl)pyrazolidin-3-one

: 1284183-81-8
tert-butyl 5-(4-(3-(2-(methoxy(methoxycarbonyl)amino)benzyloxy)-1H-pyrazol-1-yl)phenylthio)pentanoate

Guidance literature:: Multi-step reaction with 3 steps

1: oxygen; copper(l) chloride / N,N-dimethyl-formamide / 5 h

2: copper(l) iodide; potassium carbonate; ethylene glycol / isopropyl alcohol / 24 h / 80 - 85 °C / Sealed tube

3: caesium carbonate / N,N-dimethyl-formamide / 20 °C / Inert atmosphere

With copper(l) iodide; oxygen; potassium carbonate; caesium carbonate; ethylene glycol; copper(l) chloride; In N,N-dimethyl-formamide; isopropyl alcohol;
DOI:10.1039/c0ob00686f

Reference yield:

: 151827-82-6
methyl N-(2-methylphenyl)-N-methoxy-carbamate

: 1284183-81-8
tert-butyl 5-(4-(3-(2-(methoxy(methoxycarbonyl)amino)benzyloxy)-1H-pyrazol-1-yl)phenylthio)pentanoate

Guidance literature:: Multi-step reaction with 2 steps

1: N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile) / tetrachloromethane / Reflux

2: caesium carbonate / N,N-dimethyl-formamide / 20 °C / Inert atmosphere

With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); caesium carbonate; In tetrachloromethane; N,N-dimethyl-formamide;
DOI:10.1039/c0ob00686f