2-Acetamido-4,6-O-benzyliden-2-desoxy-1-N-(p-nitrobenzyliden)-β-D-glucopyranosylamin-N-oxid

Base Information

Chemical Name:2-Acetamido-4,6-O-benzyliden-2-desoxy-1-N-(p-nitrobenzyliden)-β-D-glucopyranosylamin-N-oxid
CAS No.:105874-60-0
Molecular Formula:C₂₂H₂₃N₃O₈
Molecular Weight:457.44
Hs Code.:

Synonyms:2-Acetamido-4,6-O-benzyliden-2-desoxy-1-N-(p-nitrobenzyliden)-β-D-glucopyranosylamin-N-oxid

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Chemical Property of 2-Acetamido-4,6-O-benzyliden-2-desoxy-1-N-(p-nitrobenzyliden)-β-D-glucopyranosylamin-N-oxid

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Technology Process of 2-Acetamido-4,6-O-benzyliden-2-desoxy-1-N-(p-nitrobenzyliden)-β-D-glucopyranosylamin-N-oxid

There total 2 articles about 2-Acetamido-4,6-O-benzyliden-2-desoxy-1-N-(p-nitrobenzyliden)-β-D-glucopyranosylamin-N-oxid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 555-16-8
4-nitrobenzaldehdye

: 105874-58-6
2-Acetamido-4,6-O-benzyliden-2-desoxy-D-glucose-oxim

: 105874-60-0
2-Acetamido-4,6-O-benzyliden-2-desoxy-1-N-(p-nitrobenzyliden)-β-D-glucopyranosylamin-N-oxid

Guidance literature:: toluene-4-sulfonic acid; In dimethyl sulfoxide; Ambient temperature;
DOI:10.1002/hlca.19860690526

Reference yield:

: 28297-52-1,29776-43-0,52050-06-3,135637-06-8
2-acetamido-4,6-O-benzylidene-2-deoxy-D-glucopyranose

: 105874-60-0
2-Acetamido-4,6-O-benzyliden-2-desoxy-1-N-(p-nitrobenzyliden)-β-D-glucopyranosylamin-N-oxid

Guidance literature:: Multi-step reaction with 2 steps

1: NaOEt, NH₂OH*HCl / ethanol / 50 °C / pH 7

2: 84 percent / TsOH*H₂O / dimethylsulfoxide / Ambient temperature

With hydroxylamine hydrochloride; sodium ethanolate; toluene-4-sulfonic acid; In ethanol; dimethyl sulfoxide;
DOI:10.1002/hlca.19860690526