C₅₄H₆₆N₈O₇

Base Information

Chemical Name:C₅₄H₆₆N₈O₇
CAS No.:1613056-65-7
Molecular Formula:C₅₄H₆₆N₈O₇
Molecular Weight:939.167
Hs Code.:

C<sub>54</sub>H<sub>66</sub>N<sub>8</sub>O<sub>7</sub>

Synonyms:C₅₄H₆₆N₈O₇

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Chemical Property of C₅₄H₆₆N₈O₇

Chemical Property:

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Technology Process of C₅₄H₆₆N₈O₇

There total 29 articles about C₅₄H₆₆N₈O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: C₃₄H₃₆N₆O*4ClH

: 750594-88-8
(S)-2-cyclohexyl-2-((methoxycarbonyl)amino)acetic acid

: 1613056-65-7
C₅₄H₆₆N₈O₇

Guidance literature:: With 1-hydroxy-7-aza-benzotriazole; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In dichloromethane; at 0 - 20 ℃; for 3h; Inert atmosphere; Sealed tube;

Reference yield:

: 1228968-97-5
2(S)-2-(5-trimethylsilanylethynyl-1H-imidazo1-2-yl)pyrrolidine-1-carboxylic acid tert-butyl ester

: 1613056-65-7
C₅₄H₆₆N₈O₇

Guidance literature:: Multi-step reaction with 5 steps

1: potassium carbonate / methanol; tetrahydrofuran / 6 h / 20 °C / Inert atmosphere; Sealed tube

2: triethylamine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triphenylphosphine / N,N-dimethyl-formamide / 6.16 h / 20 - 90 °C / Inert atmosphere; Sealed tube

3: potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / water; 1,2-dimethoxyethane / 4 h / 90 °C / Inert atmosphere; Sealed tube

4: hydrogenchloride / ethyl acetate / 8 h / 20 °C / Inert atmosphere; Sealed tube

5: N-ethyl-N,N-diisopropylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 1-hydroxy-7-aza-benzotriazole / dichloromethane / 3 h / 0 - 20 °C / Inert atmosphere; Sealed tube

With hydrogenchloride; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; 1-hydroxy-7-aza-benzotriazole; potassium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-ethyl-N,N-diisopropylamine; triphenylphosphine; In tetrahydrofuran; methanol; 1,2-dimethoxyethane; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide;

Reference yield:

: 1228968-98-6
(S)-2-(5-ethynyl-1H-imidazol-2-yl)pyrrolidine-1-carboxylic acid tert-butyl ester

: 1613056-65-7
C₅₄H₆₆N₈O₇

Guidance literature:: Multi-step reaction with 4 steps

1: triethylamine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triphenylphosphine / N,N-dimethyl-formamide / 6.16 h / 20 - 90 °C / Inert atmosphere; Sealed tube

2: potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / water; 1,2-dimethoxyethane / 4 h / 90 °C / Inert atmosphere; Sealed tube

3: hydrogenchloride / ethyl acetate / 8 h / 20 °C / Inert atmosphere; Sealed tube

4: N-ethyl-N,N-diisopropylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 1-hydroxy-7-aza-benzotriazole / dichloromethane / 3 h / 0 - 20 °C / Inert atmosphere; Sealed tube

With hydrogenchloride; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; 1-hydroxy-7-aza-benzotriazole; potassium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-ethyl-N,N-diisopropylamine; triphenylphosphine; In 1,2-dimethoxyethane; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide;