1-<2-ethyl>-3-piperidinemethanol

Base Information

Chemical Name:1-<2-ethyl>-3-piperidinemethanol
CAS No.:143747-56-2
Molecular Formula:C₂₁H₂₅Cl₂NO₂
Molecular Weight:394.341
Hs Code.:

1-<2-<bis(4-chlorophenyl)methoxy>ethyl>-3-piperidinemethanol

Synonyms:1-<2-ethyl>-3-piperidinemethanol

Suppliers and Price of 1-<2-ethyl>-3-piperidinemethanol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-<2-ethyl>-3-piperidinemethanol

Chemical Property:

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Technology Process of 1-<2-ethyl>-3-piperidinemethanol

There total 4 articles about 1-<2-ethyl>-3-piperidinemethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 110283-43-7
1-<2-ethyl>-3-piperidinecarboxylic acid ethyl ester

: 143747-56-2
1-<2-ethyl>-3-piperidinemethanol

Guidance literature:: With diisobutylaluminium hydride; In hexane; dichloromethane; at -70 - 20 ℃; for 16h;
DOI:10.1021/jm00100a032

Reference yield:

: 90-97-1
4,4'-dichlorobenzophenone

: 143747-56-2
1-<2-ethyl>-3-piperidinemethanol

Guidance literature:: Multi-step reaction with 3 steps

1: conc. H₂SO₄ / toluene / 2 h / 85 - 90 °C

2: K₂CO₃ / acetonitrile / 15 h / Heating

3: 2.18 g / diisobutylaluminum hydride / CH₂Cl₂; hexane / 16 h / -70 - 20 °C

With sulfuric acid; diisobutylaluminium hydride; potassium carbonate; In hexane; dichloromethane; toluene; acetonitrile;
DOI:10.1021/jm00100a032

Reference yield:

: 221916-05-8
1-bromo-2-[bis(4-chlorophenyl)methoxy]ethane

: 143747-56-2
1-<2-ethyl>-3-piperidinemethanol

Guidance literature:: Multi-step reaction with 2 steps

1: K₂CO₃ / acetonitrile / 15 h / Heating

2: 2.18 g / diisobutylaluminum hydride / CH₂Cl₂; hexane / 16 h / -70 - 20 °C

With diisobutylaluminium hydride; potassium carbonate; In hexane; dichloromethane; acetonitrile;
DOI:10.1021/jm00100a032