methyl 2-{[(4-fluorophenyl)methyl]oxy}-5-[(1Z)-3-oxo-1-propen-1-yl]benzoate

Base Information

Chemical Name:methyl 2-{[(4-fluorophenyl)methyl]oxy}-5-[(1Z)-3-oxo-1-propen-1-yl]benzoate
CAS No.:1285517-58-9
Molecular Formula:C₁₈H₁₅FO₄
Molecular Weight:314.313
Hs Code.:

Synonyms:methyl 2-{[(4-fluorophenyl)methyl]oxy}-5-[(1Z)-3-oxo-1-propen-1-yl]benzoate

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Chemical Property of methyl 2-{[(4-fluorophenyl)methyl]oxy}-5-[(1Z)-3-oxo-1-propen-1-yl]benzoate

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Technology Process of methyl 2-{[(4-fluorophenyl)methyl]oxy}-5-[(1Z)-3-oxo-1-propen-1-yl]benzoate

There total 3 articles about methyl 2-{[(4-fluorophenyl)methyl]oxy}-5-[(1Z)-3-oxo-1-propen-1-yl]benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3054-95-3
acrylaldehyde diethyl acetal

: 1285517-41-0
methyl 2-{[(4-fluorophenyl)methyl]oxy}-5-iodobenzoate

: 1285517-58-9
methyl 2-{[(4-fluorophenyl)methyl]oxy}-5-[(1Z)-3-oxo-1-propen-1-yl]benzoate

Guidance literature:: acrylaldehyde diethyl acetal; methyl 2-{[(4-fluorophenyl)methyl]oxy}-5-iodobenzoate; With potassium carbonate; palladium diacetate; In N,N-dimethyl-formamide; at 120 ℃; for 0.666667h; microwave irradiation;

With hydrogenchloride; water; In N,N-dimethyl-formamide; for 0.333333h; Cooling;

Reference yield:

: 459-46-1
4-Fluorobenzyl bromide

: 1285517-58-9
methyl 2-{[(4-fluorophenyl)methyl]oxy}-5-[(1Z)-3-oxo-1-propen-1-yl]benzoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium carbonate / acetone / Reflux

2.1: potassium carbonate / palladium diacetate / N,N-dimethyl-formamide / 0.67 h / 120 °C / microwave irradiation

2.2: 0.33 h / Cooling

With potassium carbonate; palladium diacetate; In N,N-dimethyl-formamide; acetone;

Reference yield:

: 4068-75-1
methyl 5-iodosalicylate

: 1285517-58-9
methyl 2-{[(4-fluorophenyl)methyl]oxy}-5-[(1Z)-3-oxo-1-propen-1-yl]benzoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium carbonate / acetone / Reflux

2.1: potassium carbonate / palladium diacetate / N,N-dimethyl-formamide / 0.67 h / 120 °C / microwave irradiation

2.2: 0.33 h / Cooling

With potassium carbonate; palladium diacetate; In N,N-dimethyl-formamide; acetone;