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C20H19FN4O4S2

Base Information
  • Chemical Name:C20H19FN4O4S2
  • CAS No.:1310839-78-1
  • Molecular Formula:C20H19FN4O4S2
  • Molecular Weight:462.526
  • Hs Code.:
C<sub>20</sub>H<sub>19</sub>FN<sub>4</sub>O<sub>4</sub>S<sub>2</sub>

Synonyms:C20H19FN4O4S2

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Chemical Property of C20H19FN4O4S2
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Technology Process of C20H19FN4O4S2

There total 13 articles about C20H19FN4O4S2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With sulfuric acid; at 20 ℃; for 15.5h;
Guidance literature:
Multi-step reaction with 13 steps
1.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / ethyl acetate / 3 h / 20 °C / Reflux
1.2: 1.5 h / 20 °C
2.1: sodium hypochlorite / dichloromethane; water / 0.5 h / 20 °C
3.1: n-butyllithium / toluene; hexane; tetrahydrofuran / 0.5 h / -70 °C / Inert atmosphere
3.2: 0.42 h / -70 °C / Inert atmosphere
3.3: 1.25 h / -70 °C / Inert atmosphere
4.1: nitric acid; sulfuric acid / 1 h / Cooling with ice
5.1: ammonium chloride; iron / ethanol; water / 2 h / 20 - 45 °C
6.1: triethylamine / methanol / 4 h / 20 °C
7.1: hydrogen / 5% rhodium-on-charcoal / ethanol / 23 h / 20 °C
8.1: tetrahydrofuran / 14 h / 20 - 70 °C
9.1: potassium carbonate / water; tetrahydrofuran; methanol / 5.5 h / 20 - 50 °C
10.1: triethylamine / water; tetrahydrofuran / 4.5 h / 20 °C / Cooling with ice
11.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / ethyl acetate / 6 h / 20 °C / Reflux
11.2: 2 h / 20 °C
12.1: acetone / 0.83 h / 20 °C / Cooling with ice
13.1: sulfuric acid / 15.5 h / 20 °C
With sodium hypochlorite; n-butyllithium; sulfuric acid; hydrogen; nitric acid; iron; potassium carbonate; ammonium chloride; triethylamine; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; 5% rhodium-on-charcoal; In tetrahydrofuran; methanol; ethanol; hexane; dichloromethane; water; ethyl acetate; acetone; toluene;
Guidance literature:
Multi-step reaction with 12 steps
1.1: sodium hypochlorite / dichloromethane; water / 0.5 h / 20 °C
2.1: n-butyllithium / toluene; hexane; tetrahydrofuran / 0.5 h / -70 °C / Inert atmosphere
2.2: 0.42 h / -70 °C / Inert atmosphere
2.3: 1.25 h / -70 °C / Inert atmosphere
3.1: nitric acid; sulfuric acid / 1 h / Cooling with ice
4.1: ammonium chloride; iron / ethanol; water / 2 h / 20 - 45 °C
5.1: triethylamine / methanol / 4 h / 20 °C
6.1: hydrogen / 5% rhodium-on-charcoal / ethanol / 23 h / 20 °C
7.1: tetrahydrofuran / 14 h / 20 - 70 °C
8.1: potassium carbonate / water; tetrahydrofuran; methanol / 5.5 h / 20 - 50 °C
9.1: triethylamine / water; tetrahydrofuran / 4.5 h / 20 °C / Cooling with ice
10.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / ethyl acetate / 6 h / 20 °C / Reflux
10.2: 2 h / 20 °C
11.1: acetone / 0.83 h / 20 °C / Cooling with ice
12.1: sulfuric acid / 15.5 h / 20 °C
With sodium hypochlorite; n-butyllithium; sulfuric acid; hydrogen; nitric acid; iron; potassium carbonate; ammonium chloride; triethylamine; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; 5% rhodium-on-charcoal; In tetrahydrofuran; methanol; ethanol; hexane; dichloromethane; water; ethyl acetate; acetone; toluene;
upstream raw materials:

6-hepten-1-ol

hept-6-enal oxime

C13H16FNO

C13H15FN2O3

Downstream raw materials:

C14H16FN3S

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