(E)-3-Hydroxy-5-(4-methoxy-phenylsulfanyl)-2-methyl-pent-4-enoic acid (E)-3-methoxycarbonyl-allyl ester

Base Information

Chemical Name:(E)-3-Hydroxy-5-(4-methoxy-phenylsulfanyl)-2-methyl-pent-4-enoic acid (E)-3-methoxycarbonyl-allyl ester
CAS No.:192520-05-1
Molecular Formula:C₁₈H₂₂O₆S
Molecular Weight:366.435
Hs Code.:

Synonyms:(E)-3-Hydroxy-5-(4-methoxy-phenylsulfanyl)-2-methyl-pent-4-enoic acid (E)-3-methoxycarbonyl-allyl ester

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Chemical Property of (E)-3-Hydroxy-5-(4-methoxy-phenylsulfanyl)-2-methyl-pent-4-enoic acid (E)-3-methoxycarbonyl-allyl ester

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Technology Process of (E)-3-Hydroxy-5-(4-methoxy-phenylsulfanyl)-2-methyl-pent-4-enoic acid (E)-3-methoxycarbonyl-allyl ester

There total 3 articles about (E)-3-Hydroxy-5-(4-methoxy-phenylsulfanyl)-2-methyl-pent-4-enoic acid (E)-3-methoxycarbonyl-allyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 192520-04-0
(E)-4-(2-Bromo-propionyloxy)-but-2-enoic acid methyl ester

: 192519-98-5
(E)-3-(4-Methoxy-phenylsulfanyl)-propenal

: 192520-05-1
(E)-3-Hydroxy-5-(4-methoxy-phenylsulfanyl)-2-methyl-pent-4-enoic acid (E)-3-methoxycarbonyl-allyl ester

Guidance literature:: With zinc; In tetrahydrofuran; at 55 ℃; for 1h; Irradiation;
DOI:10.1016/S0040-4020(97)00606-6

Reference yield:

: (E)-3-(4-Methoxy-phenylsulfanyl)-prop-2-en-1-ol

: 192520-05-1
(E)-3-Hydroxy-5-(4-methoxy-phenylsulfanyl)-2-methyl-pent-4-enoic acid (E)-3-methoxycarbonyl-allyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: iodobenzoic acid / dimethylsulfoxide; tetrahydrofuran / 0.5 h / 20 °C

2: 67 percent / Zn / tetrahydrofuran / 1 h / 55 °C / Irradiation

With 2-Iodobenzoic acid; zinc; In tetrahydrofuran; dimethyl sulfoxide;
DOI:10.1016/S0040-4020(97)00606-6

Reference yield:

: 29576-13-4
methyl 4-hydroxy-2-butenoate

: 192520-05-1
(E)-3-Hydroxy-5-(4-methoxy-phenylsulfanyl)-2-methyl-pent-4-enoic acid (E)-3-methoxycarbonyl-allyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 88 percent / pyridine / CH₂Cl₂ / 0.17 h / 20 °C

2: 67 percent / Zn / tetrahydrofuran / 1 h / 55 °C / Irradiation

With pyridine; zinc; In tetrahydrofuran; dichloromethane;
DOI:10.1016/S0040-4020(97)00606-6