N-(2,6-difluorobenzoyl)-N-(2,6-difluorobenzyl)-5-chloro-2-nitroaniline

Base Information

Chemical Name:N-(2,6-difluorobenzoyl)-N-(2,6-difluorobenzyl)-5-chloro-2-nitroaniline
CAS No.:212504-08-0
Molecular Formula:C₂₀H₁₁ClF₄N₂O₃
Molecular Weight:438.766
Hs Code.:

Synonyms:N-(2,6-difluorobenzoyl)-N-(2,6-difluorobenzyl)-5-chloro-2-nitroaniline

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(2,6-difluorobenzoyl)-N-(2,6-difluorobenzyl)-5-chloro-2-nitroaniline

Chemical Property:

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Technology Process of N-(2,6-difluorobenzoyl)-N-(2,6-difluorobenzyl)-5-chloro-2-nitroaniline

There total 3 articles about N-(2,6-difluorobenzoyl)-N-(2,6-difluorobenzyl)-5-chloro-2-nitroaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 212503-98-5
N-(2,6-difluorobenzoyl)-5-chloro-2-nitroaniline

: 85118-00-9
2,6-Difluorobenzyl bromide

: 212504-08-0
N-(2,6-difluorobenzoyl)-N-(2,6-difluorobenzyl)-5-chloro-2-nitroaniline

Guidance literature:: With sodium hydride; In tetrahydrofuran; for 8h;
DOI:10.1021/jm060103d

Reference yield:

: 212503-97-4
N,N-bis-(2,6-difluorobenzoyl)-5-chloro-2-nitroaniline

: 212504-08-0
N-(2,6-difluorobenzoyl)-N-(2,6-difluorobenzyl)-5-chloro-2-nitroaniline

Guidance literature:: Multi-step reaction with 2 steps

1: 84 percent / NaOH / methanol; dioxane / 0.75 h / 20 °C

2: 75 percent / NaH / tetrahydrofuran / 8 h

With sodium hydroxide; sodium hydride; In tetrahydrofuran; 1,4-dioxane; methanol;
DOI:10.1021/jm060103d

Reference yield:

: 1635-61-6
5-chloro-2-nitroaniline

: 212504-08-0
N-(2,6-difluorobenzoyl)-N-(2,6-difluorobenzyl)-5-chloro-2-nitroaniline

Guidance literature:: Multi-step reaction with 3 steps

1: 93 percent / pyridine / tetrahydrofuran / 20 °C

2: 84 percent / NaOH / methanol; dioxane / 0.75 h / 20 °C

3: 75 percent / NaH / tetrahydrofuran / 8 h

With pyridine; sodium hydroxide; sodium hydride; In tetrahydrofuran; 1,4-dioxane; methanol;
DOI:10.1021/jm060103d