(3-cyano-1,5-dimethylcyclohexa-2,5-dienyl)carbaminic acid tert-butyl ester

Base Information

Chemical Name:(3-cyano-1,5-dimethylcyclohexa-2,5-dienyl)carbaminic acid tert-butyl ester
CAS No.:866918-71-0
Molecular Formula:C₁₄H₂₀N₂O₂
Molecular Weight:248.325
Hs Code.:

Synonyms:(3-cyano-1,5-dimethylcyclohexa-2,5-dienyl)carbaminic acid tert-butyl ester

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Chemical Property of (3-cyano-1,5-dimethylcyclohexa-2,5-dienyl)carbaminic acid tert-butyl ester

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Technology Process of (3-cyano-1,5-dimethylcyclohexa-2,5-dienyl)carbaminic acid tert-butyl ester

There total 2 articles about (3-cyano-1,5-dimethylcyclohexa-2,5-dienyl)carbaminic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: (5-cyano-1,3-dimethyl-6-nitrocyclohex-2-enyl)carbamic acid tert-butyl ester

: 866918-71-0
(3-cyano-1,5-dimethylcyclohexa-2,5-dienyl)carbaminic acid tert-butyl ester

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undecane-4-ene; In diethyl ether; for 1h; Heating;
DOI:10.1002/anie.200463032

Reference yield:

: 866918-66-3
E-(1,3-dimethylbuta-1,3-dienyl)carbamic acid tert-butyl ester

: 866918-71-0
(3-cyano-1,5-dimethylcyclohexa-2,5-dienyl)carbaminic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 88 percent / benzene / 0.75 h / 0 - 20 °C

2: 69 percent / 1,8-diazabicyclo[5.4.0]undec-4-ene / diethyl ether / 1 h / Heating

With 1,8-diazabicyclo[5.4.0]undecane-4-ene; In diethyl ether; benzene; 1: Diels-Alder reaction;
DOI:10.1002/anie.200463032