Diisopropyl 4-[(diisopropoxyphosphoryl)methylphenyl]difluoromethylphosphonate

Base Information

Chemical Name:Diisopropyl 4-[(diisopropoxyphosphoryl)methylphenyl]difluoromethylphosphonate
CAS No.:263165-18-0
Molecular Formula:C₂₀H₃₄F₂O₆P₂
Molecular Weight:470.431
Hs Code.:

Synonyms:Diisopropyl 4-[(diisopropoxyphosphoryl)methylphenyl]difluoromethylphosphonate

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Chemical Property of Diisopropyl 4-[(diisopropoxyphosphoryl)methylphenyl]difluoromethylphosphonate

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Technology Process of Diisopropyl 4-[(diisopropoxyphosphoryl)methylphenyl]difluoromethylphosphonate

There total 4 articles about Diisopropyl 4-[(diisopropoxyphosphoryl)methylphenyl]difluoromethylphosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 691-96-3
diisopropyl phosphite

: 263165-16-8
Diisopropyl 4-(chloromethylphenyl)difluoromethylphosphonate

: 263165-18-0
Diisopropyl 4-[(diisopropoxyphosphoryl)methylphenyl]difluoromethylphosphonate

Guidance literature:: With sodium hydride; In tetrahydrofuran; at 20 ℃;
DOI:10.1039/a906507e

Reference yield:

: 513-02-0
triisopropyl phosphate

: 263165-18-0
Diisopropyl 4-[(diisopropoxyphosphoryl)methylphenyl]difluoromethylphosphonate

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / CH₂Cl₂ / 2 h / 20 °C

2: 73 percent / DAST / CH₂Cl₂ / 14 h / 20 °C

3: 90 percent / sodium hydride / tetrahydrofuran / 20 °C

With sodium hydride; 4,4'-diaminostilbene-2,2'-disulfonic acid; In tetrahydrofuran; dichloromethane; 1: Substitution / 2: Substitution / 3: Substitution;
DOI:10.1039/a906507e

Reference yield:

: 876-08-4
p-(chloromethyl)benzoyl chloride

: 263165-18-0
Diisopropyl 4-[(diisopropoxyphosphoryl)methylphenyl]difluoromethylphosphonate

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / CH₂Cl₂ / 2 h / 20 °C

2: 73 percent / DAST / CH₂Cl₂ / 14 h / 20 °C

3: 90 percent / sodium hydride / tetrahydrofuran / 20 °C

With sodium hydride; 4,4'-diaminostilbene-2,2'-disulfonic acid; In tetrahydrofuran; dichloromethane; 1: Substitution / 2: Substitution / 3: Substitution;
DOI:10.1039/a906507e