methyl 2-O-benzoyl-6,7-O-(1,1,3,3-tetraisopropyl-1,3-disiloxane-1,3-diyl)-L-glycero-α-D-manno-heptopyranoside

Base Information

Chemical Name:methyl 2-O-benzoyl-6,7-O-(1,1,3,3-tetraisopropyl-1,3-disiloxane-1,3-diyl)-L-glycero-α-D-manno-heptopyranoside
CAS No.:1520094-76-1
Molecular Formula:C₂₇H₄₆O₉Si₂
Molecular Weight:570.828
Hs Code.:

Synonyms:methyl 2-O-benzoyl-6,7-O-(1,1,3,3-tetraisopropyl-1,3-disiloxane-1,3-diyl)-L-glycero-α-D-manno-heptopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 2-O-benzoyl-6,7-O-(1,1,3,3-tetraisopropyl-1,3-disiloxane-1,3-diyl)-L-glycero-α-D-manno-heptopyranoside

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Technology Process of methyl 2-O-benzoyl-6,7-O-(1,1,3,3-tetraisopropyl-1,3-disiloxane-1,3-diyl)-L-glycero-α-D-manno-heptopyranoside

There total 4 articles about methyl 2-O-benzoyl-6,7-O-(1,1,3,3-tetraisopropyl-1,3-disiloxane-1,3-diyl)-L-glycero-α-D-manno-heptopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 127642-33-5,686299-10-5
methyl L-glycero-α-D-manno-heptopyranoside

: 1520094-76-1
methyl 2-O-benzoyl-6,7-O-(1,1,3,3-tetraisopropyl-1,3-disiloxane-1,3-diyl)-L-glycero-α-D-manno-heptopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 1H-imidazole / N,N-dimethyl-formamide / 2.5 h / -55 - 20 °C

2: camphor-10-sulfonic acid / dichloromethane / 0.5 h / 20 °C

3: water / 1 h / 20 °C

With 1H-imidazole; camphor-10-sulfonic acid; water; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo402312x

Reference yield:

: 1520094-68-1
methyl 6,7-O-(1,1,3,3-tetraisopropyl-1,3-disiloxane-1,3-diyl)-Lglycero-α-D-manno-heptopyranoside

: 1520094-76-1
methyl 2-O-benzoyl-6,7-O-(1,1,3,3-tetraisopropyl-1,3-disiloxane-1,3-diyl)-L-glycero-α-D-manno-heptopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: camphor-10-sulfonic acid / dichloromethane / 0.5 h / 20 °C

2: water / 1 h / 20 °C

With camphor-10-sulfonic acid; water; In dichloromethane;
DOI:10.1021/jo402312x

Reference yield:

: 69304-37-6
1,3-Dichloro-1,1,3,3-tetraisopropyldisiloxane

: 1520094-76-1
methyl 2-O-benzoyl-6,7-O-(1,1,3,3-tetraisopropyl-1,3-disiloxane-1,3-diyl)-L-glycero-α-D-manno-heptopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 1H-imidazole / N,N-dimethyl-formamide / 2.5 h / -55 - 20 °C

2: camphor-10-sulfonic acid / dichloromethane / 0.5 h / 20 °C

3: water / 1 h / 20 °C

With 1H-imidazole; camphor-10-sulfonic acid; water; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo402312x