1-benzyl-2-methylpyrrolidine hydrochloride

Base Information

Chemical Name:1-benzyl-2-methylpyrrolidine hydrochloride
CAS No.:91562-57-1
Molecular Formula:C₁₂H₁₇N*ClH
Molecular Weight:211.735
Hs Code.:

Synonyms:1-benzyl-2-methylpyrrolidine hydrochloride

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Chemical Property of 1-benzyl-2-methylpyrrolidine hydrochloride

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Technology Process of 1-benzyl-2-methylpyrrolidine hydrochloride

There total 5 articles about 1-benzyl-2-methylpyrrolidine hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 448957-53-7
N-benzyl-4-hydroxypentylamine

: 91562-57-1
1-benzyl-2-methylpyrrolidine hydrochloride

Guidance literature:: N-benzyl-4-hydroxypentylamine; With N,N-dimethylacetamide dimethyl acetal; tin(IV) chloride; In dichloromethane; at 20 ℃; for 5h; Inert atmosphere;

With hydrogenchloride; In 1,4-dioxane; dichloromethane; at 20 ℃; for 0.0833333h; Inert atmosphere;
DOI:10.1039/c4ra10625c

Reference yield: 89.0%

: C₁₂H₁₉NO*ClH

: 91562-57-1
1-benzyl-2-methylpyrrolidine hydrochloride

Guidance literature:: With N,N-dimethylacetamide dimethyl acetal; In 1,2-dichloro-ethane; for 16h; Inert atmosphere; Molecular sieve; Reflux;
DOI:10.1039/c4ra10625c

Reference yield:

: 108-29-2
5-methyl-dihydro-furan-2-one

: 91562-57-1
1-benzyl-2-methylpyrrolidine hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1.1: benzene / 12 h / Inert atmosphere; Reflux

2.1: lithium aluminium tetrahydride / tetrahydrofuran / 18.5 h / 0 °C / Inert atmosphere; Reflux

3.1: N,N-dimethylacetamide dimethyl acetal; tin(IV) chloride / dichloromethane / 5 h / 20 °C / Inert atmosphere

3.2: 0.08 h / 20 °C / Inert atmosphere

With lithium aluminium tetrahydride; N,N-dimethylacetamide dimethyl acetal; tin(IV) chloride; In tetrahydrofuran; dichloromethane; benzene;
DOI:10.1039/c4ra10625c