(+)-11α-acetylthio-11-deoxy-11α-homoprostaglandin F_2β 15-acetate methyl ester

Base Information

• Chemical Name: (+)-11α-acetylthio-11-deoxy-11α-homoprostaglandin F_2β 15-acetate methyl ester
• CAS No.: 89617-00-5
• Molecular Formula: C₂₆H₄₂O₆S
• Molecular Weight: 482.682

Synonyms:(+)-11α-acetylthio-11-deoxy-11α-homoprostaglandin F_2β 15-acetate methyl ester

Chemical Property of (+)-11α-acetylthio-11-deoxy-11α-homoprostaglandin F_2β 15-acetate methyl ester

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of (+)-11α-acetylthio-11-deoxy-11α-homoprostaglandin F_2β 15-acetate methyl ester

There total 31 articles about (+)-11α-acetylthio-11-deoxy-11α-homoprostaglandin F_2β 15-acetate methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

(Z)-7-[(1R,2R,4S)-2-((E)-3-Acetoxy-oct-1-enyl)-4-acetylsulfanyl-6-oxo-cyclohexyl]-hept-5-enoic acid methyl ester (81755-82-0,89616-99-9) → (Z)-7-[(1R,2R,4S,6R)-2-((E)-3-Acetoxy-oct-1-enyl)-4-acetylsulfanyl-6-hydroxy-cyclohexyl]-hept-5-enoic acid methyl ester (89560-32-7,89617-00-5) + (Z)-7-[(1R,2R,4S,6S)-2-((E)-3-Acetoxy-oct-1-enyl)-4-acetylsulfanyl-6-hydroxy-cyclohexyl]-hept-5-enoic acid methyl ester (89560-32-7,89617-00-5)

Guidance literature:

With zinc(II) tetrahydroborate; In 1,2-dimethoxyethane; at 0 ℃;

DOI:10.1016/S0040-4039(01)92486-4

Reference yield: 46.0%

(Z)-7-[(1R,2R,4S)-2-((E)-3-Acetoxy-oct-1-enyl)-4-acetylsulfanyl-6-oxo-cyclohexyl]-hept-5-enoic acid methyl ester (81755-82-0,89616-99-9) → (Z)-7-[(1R,2R,4S,6R)-2-((E)-3-Acetoxy-oct-1-enyl)-4-acetylsulfanyl-6-hydroxy-cyclohexyl]-hept-5-enoic acid methyl ester (89560-32-7,89617-00-5) + (Z)-7-[(1R,2R,4S,6S)-2-((E)-3-Acetoxy-oct-1-enyl)-4-acetylsulfanyl-6-hydroxy-cyclohexyl]-hept-5-enoic acid methyl ester (89560-32-7,89617-00-5)

Guidance literature:

With zinc(II) tetrahydroborate; In 1,2-dimethoxyethane; at 0 ℃;

DOI:10.1016/S0040-4039(01)92486-4

Reference yield: 24.0%

(Z)-7-[(1R,2R,4S)-2-((E)-3-Acetoxy-oct-1-enyl)-4-acetylsulfanyl-6-oxo-cyclohexyl]-hept-5-enoic acid methyl ester (81755-82-0,89616-99-9) → (Z)-7-[(1R,2R,4S,6S)-2-((E)-3-Acetoxy-oct-1-enyl)-4-acetylsulfanyl-6-hydroxy-cyclohexyl]-hept-5-enoic acid methyl ester (89560-32-7,89617-00-5)

Guidance literature:

With zinc(II) tetrahydroborate; In 1,2-dimethoxyethane; at 0 ℃;

DOI:10.1016/S0040-4039(01)92486-4

upstream raw materials:

(Z)-7-[(1R,2R,4S)-2-((E)-3-Acetoxy-oct-1-enyl)-4-acetylsulfanyl-6-oxo-cyclohexyl]-hept-5-enoic acid methyl ester

PGE₂ methyl ester

(Z)-7-[(1R,2R)-2-((E)-3-Acetoxy-oct-1-enyl)-5-oxo-cyclopentyl]-hept-5-enoic acid methyl ester

(4R,5R)-4-((E)-3-Acetoxy-oct-1-enyl)-5-((Z)-6-methoxycarbonyl-hex-2-enyl)-6-oxo-cyclohex-1-enecarboxylic acid ethyl ester

Downstream raw materials:

(Z)-7-[(1R,2R,4S,6R)-2-((E)-3-Acetoxy-oct-1-enyl)-4-acetylsulfanyl-6-methanesulfonyloxy-cyclohexyl]-hept-5-enoic acid methyl ester

(+)-(9,11)-Epithia-(11,12)-methano-thromboxane A₂

(Z)-7-[(1R,2R,4S)-2-((E)-3-Acetoxy-oct-1-enyl)-4-acetylsulfanyl-6-oxo-cyclohexyl]-hept-5-enoic acid methyl ester

(Z)-7-[(1R,2R,4S,6R)-2-((E)-3-Acetoxy-oct-1-enyl)-4-acetylsulfanyl-6-hydroxy-cyclohexyl]-hept-5-enoic acid methyl ester

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